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C1CC2=CC=CC=C2C1COChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2,3-dihydro-1H-inden-1-ylmethanol |
|---|---|
| IUPAC Name | — |
| CAS Number | 1196-17-4 |
| Database ID | 271880 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2,3-dihydro-1H-inden-1-ylmethanol (CAS 1196-17-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 271880
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-0e1f8eb3286a45b2a87e934af782fe08Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b1b0bd7ab9d7478c82ba906961ea3343Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-f0b3299226134fa3b5a5a53b9cb8c5d8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added drop-wise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound 1a as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-ceefa9f4b4bc4e18a5d22a4e0ada0050Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added drop-wise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound 1a as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-ceefa9f4b4bc4e18a5d22a4e0ada0050Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added drop-wise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound 1a as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-ceefa9f4b4bc4e18a5d22a4e0ada0050Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-0e1f8eb3286a45b2a87e934af782fe08Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b1b0bd7ab9d7478c82ba906961ea3343Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added dropwise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound la as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-60f3fcc1123f4febab62bcec7f8cf5afConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added dropwise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound la as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-60f3fcc1123f4febab62bcec7f8cf5afConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added dropwise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound 1a as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-684cbecae7f7467db6a5a55c3aa1bd63Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a suspension of LiAlH4 (4.7 g) in diethyl ether (200 ml) was added dropwise a solution of AlCl3 in diethyl ether (200 ml). A solution of 1-indanecarboxylic acid (10 g) (prepared according to the method of Hansen et al. Helv. Chim. Acta 1982, 33, 325-343) in dry tetrahydrofuran (200 ml) was added dropwise at 10-15° C. The mixture was finally stirred at room temperature for 1.5 hours. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C. Precipitated inorganic salts were filtered off and the solvents evaporated in vacuo leaving 6.8 g of the title compound 1a as a viscous oil which was used without further purification. Excess AlH3 was destroyed by addition of concentrated aqueous NaOH solution (25 ml) at 0° C Precipitated inorganic salts were filtered off the solvents evaporated in vacuo
Source ID: ord-684cbecae7f7467db6a5a55c3aa1bd63PubChem References
These sources are listed in the compound's public database record.
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