01
Reaction #1136821
Reaction scheme
No renderable structure data available
No renderable structure data available
No renderable structure data available
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04579969
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture consisting of 18.1 g of α,α-dimethylbenzyl-isocyanate and 14.2 g of 2-chlorobenzylamine was allowed to stand for 2 hours at room temperature. The white deposit formed was then filtered off. Washing with n-hexane and recrystallization from ethanol gave 28.5 g of colorless crystal product, m.p. 165°-166° C. The white deposit formed was then filtered off Washing with n-hexane and recrystallization from ethanol
Source ID: ord-be49908a3d954b5b89eb40641c730788