1-[4-(aminomethyl)phenyl]-3-methylbutan-1-one

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Use a method similar to the General Procedure 1-3, using 7-chloro-3-(2,2,2-trifluoroacetyl)-6-trifluoromethanesulfonyloxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine (175 mg, 0.42 mmol) and 4-(3-methyl-butyryl)-benzylamine (160 mg, 0.8 mmol) to obtain the title compound as a yellow syrup (85 mg, 45%). MS (ES+) m/z: 467 (M+H)+.