No renderable structure data available
CCOC1=C(C=CC(=C1)C=O)OCCOChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 3-ethoxy-4-(2-hydroxyethoxy)benzaldehyde |
|---|---|
| IUPAC Name | — |
| CAS Number | 91123-08-9 |
| Database ID | 1757953 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
3-ethoxy-4-(2-hydroxyethoxy)benzaldehyde (CAS 91123-08-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 1757953
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
9 reactions · 9 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-087bbf4510924706b0aef654e928510fConditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-432be3fd61474c40a94a443c764835b0Conditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-ea49051e365f4d99a582c0e490e6f728Conditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-ea49051e365f4d99a582c0e490e6f728Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-087bbf4510924706b0aef654e928510fConditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-5a55b43b4eb44ffa8e11dc162a1d6c15Conditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-0baaad83b32b4bc39b88f19861cabf4cConditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-432be3fd61474c40a94a443c764835b0Conditions: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2.76 ml of 2-bromoethanol and 5.40 g of potassium carbonate were added to a solution of 5 g of 3-ethoxy-4-hydroxybenzaldehyde in 150 ml of DMF. The reaction mixture was heated to 70° C. overnight and subsequently to 120° C. for a further 4 hrs. Then, the mixture was left to cool to room temperature, filtered and concentrated in a high vacuum. The crude product was isolated by extraction and purified by chromatography on silica gel. There were obtained 6.09 g of 3-ethoxy-4-(2-hydroxy-ethoxy)-benzaldehyde as a white solid. Then, the mixture was left to cool to room temperature filtered concentrated in a high vacuum The crude product was isolated by extraction purified by chromatography on silica gel
Source ID: ord-ea49051e365f4d99a582c0e490e6f728PubChem References
These sources are listed in the compound's public database record.
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