tert-butyl N-(2-oxoethyl)carbamate

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:25.01; pressure:0.00; stir:

Procedure: The product mixture was cooled to 25 °C. Filtered through a pad of celite "The celite was washed with ethyl acetate (3 x 1 mL)." The filtrate was concentrated under reduced pressure A 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.

Conditions: temp:25.01; pressure:0.00; stir:

Procedure: The product mixture was cooled to 25 °C. Filtered through a pad of celite "The celite was washed with ethyl acetate (3 x 1 mL)." The filtrate was concentrated under reduced pressure A 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.