Reaction #98234
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05413722
Conditions: temp:190.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 300 moles of decylmethylamine, 300 moles of isononyl chloride and 350 moles of 50% caustic soda, contained in a 50 gallon reactor, was heated for 6 hours at a temperature of 190° C. The organic mixture was cooled, washed with water and further purified by fractional distillation. The amination process afforded a yield of 83% decylisononylmethylamine. When nonyl chloride is used instead of isononyl chloride, the product is decylnonylmethylamine. contained in a 50 gallon reactor The organic mixture was cooled washed with water further purified by fractional distillation
Source ID: ord-81b05e676d1640e1925112e531df1c47