N-decyl-N-methyldecan-1-amine

Conditions: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: A two-liter, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-didecylmethylamine (65.49 grams, 0.21 moles), 1-bromo-3-chloropropane (33.06 grams, 0.21 moles) and methanol (250 mL). Reaction was maintained at 65° C. for six days. Methanol was removed by rotary evaporation under reduced pressure to yield an oil. To the oil was added hexane (200 mL) causing a white solid to slowly form. The solvent was decanted off from the mixture. The remaining solid dried overnight under vacuum. Yield 81.67 grams 0.17 moles, 82%). A two-liter, 3-necked, round-bottomed flask equipped with air condensers Reaction Methanol was removed by rotary evaporation under reduced pressure to yield an oil to slowly form The solvent was decanted off from the mixture The remaining solid dried overnight under vacuum

Conditions: temp:110.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In a 12-liter 3-neck round bottom reaction flask equipped with stirrer, thermometer and condenser was placed 4746 grams (15.2 moles) of didecylmethylamine and 3160.7 grams (15.9 moles) 3-chloropropyltrimethoxysilane. The solution was stirred with heating at 110° C. under a nitrogen atmosphere for 48 hours. The dark yellow/orange liquid was then placed under vacuum (5 torr), and approximately 135 mls. residual 3-chloropropyltrimethoxysilane was removed. The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product containing 50% active material. In a 12-liter 3-neck round bottom reaction flask equipped with stirrer thermometer and condenser was placed residual 3-chloropropyltrimethoxysilane was removed The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product

Conditions: temp:110.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In a 12-liter 3-neck round bottom reaction flask equipped with stirrer, thermometer and condenser was placed 4746 grams (15.2 moles) of didecylmethylamine and 3160.7 grams (15.9 moles) 3-chloropropyltrimethoxysilane. The solution was stirred with heating at 110° C. under a nitrogen atmosphere for 48 hours. The dark yellow/orange liquid was then placed under vacuum (5 torr), and approximately 135 mls. residual 3-chloropropyltrimethoxysilane was removed. The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product containing 50% active material. In a 12-liter 3-neck round bottom reaction flask equipped with stirrer thermometer and condenser was placed residual 3-chloropropyltrimethoxysilane was removed The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product

Conditions: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: A two-liter, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-didecylmethylamine (65.49 grams, 0.21 moles), 1-bromo-3-chloropropane (33.06 grams, 0.21 moles) and methanol (250 mL). Reaction was maintained at 65° C. for six days. Methanol was removed by rotary evaporation under reduced pressure to yield an oil. To the oil was added hexane (200 mL) causing a white solid to slowly form. The solvent was decanted off from the mixture. The remaining solid dried overnight under vacuum. Yield 81.67 grams 0.17 moles, 82%). A two-liter, 3-necked, round-bottomed flask equipped with air condensers Reaction Methanol was removed by rotary evaporation under reduced pressure to yield an oil to slowly form The solvent was decanted off from the mixture The remaining solid dried overnight under vacuum

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Into an autoclave equipped with a stirrer, didecylmethylamine (1 mol), dimethylcarbonate (1.5 mol) and methanol (2.0 mol) as a solvent were introduced, and a reaction was carried out at a reaction temperature of 110° C. for 12 hours to obtain a methanol solution of dimethyldidecyl ammonium methylcarbonate. To this solution, octylic acid (1 mol) was added, and by removing carbon dioxide and methanol, which were formed as byproducts, dimethyl didecylammonium/octylate (quaternary ammonium salt (B1)) was obtained. Into an autoclave equipped with a stirrer

Conditions: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: A two-liter, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-didecylmethylamine (65.49 grams, 0.21 moles), 1-bromo-3-chloropropane (33.06 grams, 0.21 moles) and methanol (250 mL). Reaction was maintained at 65° C. for six days. Methanol was removed by rotary evaporation under reduced pressure to yield an oil. To the oil was added hexane (200 mL) causing a white solid to slowly form. The solvent was decanted off from the mixture. The remaining solid dried overnight under vacuum. Yield 81.67 grams 0.17 moles, 82%). A two-liter, 3-necked, round-bottomed flask equipped with air condensers Reaction Methanol was removed by rotary evaporation under reduced pressure to yield an oil to slowly form The solvent was decanted off from the mixture The remaining solid dried overnight under vacuum

Conditions: temp:110.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In a 12-liter 3-neck round bottom reaction flask equipped with stirrer, thermometer and condenser was placed 4746 grams (15.2 moles) of didecylmethylamine and 3160.7 grams (15.9 moles) 3-chloropropyltrimethoxysilane. The solution was stirred with heating at 110° C. under a nitrogen atmosphere for 48 hours. The dark yellow/orange liquid was then placed under vacuum (5 torr), and approximately 135 mls. residual 3-chloropropyltrimethoxysilane was removed. The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product containing 50% active material. In a 12-liter 3-neck round bottom reaction flask equipped with stirrer thermometer and condenser was placed residual 3-chloropropyltrimethoxysilane was removed The remaining product was then added slowly to 7750 grams of methanol with stirring to produce a product