01
Reaction #1504731
Reaction scheme
No renderable structure data available
No renderable structure data available
No renderable structure data available
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04113734
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Equimolar mixtures of (p-chlorophenyl)-sulphonyl isocyanate and n-butylazide were dissolved at room temperature in toluene with a molar concentration of 0.6. 1-(p-chlorophenylsulphonyl)-4-n-butyl-2-tetrazolin-5-one was obtained, which was a white powder or a clear crystalline precipitate, according to whether the precipitation occurred fast or slow. The product had a melting range of 76.5°-77.5° C. The following results were obtained by elementary analysis:
Source ID: ord-0c5cdc1c4a6e45a8895707dd7a5e0ea4