No renderable structure data available
CNC(=O)CNCC(=O)NCChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-methyl-2-[[2-(methylamino)-2-oxoethyl]amino]acetamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 725686-07-7 |
| Database ID | 14518958 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-methyl-2-[[2-(methylamino)-2-oxoethyl]amino]acetamide (CAS 725686-07-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 14518958
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-77d92a7a05234497ae105853e1bbef8aConditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-357458fff450461e85baad9d35682697Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
Source ID: ord-ae480de714cb48fda70d4bcd3524d6b1Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-d7989f36f09e446187dabeec80ee1ec1Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-77d92a7a05234497ae105853e1bbef8aConditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-d7989f36f09e446187dabeec80ee1ec1Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
Source ID: ord-c4d9a121559f472e987a0ee80953a77eConditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 )br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 )br s 1H); MS (ESI) m/e 160 )M+H+). filtered concentrated in vacuo
Source ID: ord-fd06343229954c3f9c663fa1444f8be2Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of 2-(benzyl-methylcarbamoylmethyl-amino)N-methyl-acetamid (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-methyl-2-(methylcarbamoylmethyl-amino)-acetamide in quantitative yield (1.76 g). 1HNMR(CDCl3) δ 6.95(brs, 2H), 3.23(s, 4H), 2.79(d, J=4.8 Hz, 6H), 2.25(brs, 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-f9b9c85b6c9c4e33af164179c2f64ed6Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-357458fff450461e85baad9d35682697Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
Source ID: ord-ae480de714cb48fda70d4bcd3524d6b1Conditions: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
Source ID: ord-d7989f36f09e446187dabeec80ee1ec1PubChem References
These sources are listed in the compound's public database record.
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