No renderable structure data available
CCNCC(OCC)OCCChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2,2-diethoxy-N-ethylethanamine |
|---|---|
| IUPAC Name | — |
| CAS Number | 69148-92-1 |
| Database ID | 12503261 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2,2-diethoxy-N-ethylethanamine (CAS 69148-92-1) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 12503261
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
9 reactions · 9 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-da493a8a855743cb9bf495481290dd9cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Chloro-3,5-dinitrotoluene (4.32 grams; 0.02 mole), N-ethyl-N-(2,2-diethoxyethyl)amine (3.2 grams; 0.02 mole), triethylamine (2.02 grams; 0.02 mole) and toluene (100 ml) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight resulting in the formation of a precipitate. The reaction mixture was then filtered and the filtrate washed with water, dried and stripped of solvent to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)-2,6-dinitro-p-toluidine. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture was heated at reflux overnight resulting in the formation of a precipitate The reaction mixture was then filtered the filtrate washed with water dried
Source ID: ord-b9624842cc48450d8ca1d1793312fb22Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Chloro-3,5-dinitrobenzotrifluoride (5.4 grams; 0.02 mole) dissolved in toluene (50 ml) and a solution of N-ethyl-N-(2,2-diethoxyethyl)amine (3.2 grams; 0.02 mole) and triethylamine (2.02 grams; 0.02 mole in toluene (50 ml) were charged into a glass reaction vessel equipped with stirrer, thermometer and reflux condenser. The mixture was heated at reflux overnight resulting in the formation of a precipitate. The reaction mixture was then filtered and the filtrate was washed with water, dried and stripped of solvent to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)-2,6-dinitro-4-trifluoromethylaniline. equipped with stirrer thermometer and reflux condenser The mixture was heated at reflux overnight resulting in the formation of a precipitate The reaction mixture was then filtered the filtrate was washed with water dried
Source ID: ord-e06ee16277c14ee9b483fa8182be6a7cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Ethylamine (38 grams) and 1-bromo-2,2-diethoxyethane (20 grams) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight. After this time the mixture was washed with aqueous sodium hydroxide and the organic phase separated from the aqueous phase. The organic phase was then distilled to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)amine as an oil. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture was heated at reflux overnight After this time the mixture was washed with aqueous sodium hydroxide the organic phase separated from the aqueous phase The organic phase was then distilled
Source ID: ord-8bfcf25171014b779da7e48d424b7a69Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Ethylamine (38 grams) and 1-bromo-2,2-diethoxyethane (20 grams) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight. After this time the mixture was washed with aqueous sodium hydroxide and the organic phase separated from the aqueous phase. The organic phase was then distilled to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)amine as an oil. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture was heated at reflux overnight After this time the mixture was washed with aqueous sodium hydroxide the organic phase separated from the aqueous phase The organic phase was then distilled
Source ID: ord-8bfcf25171014b779da7e48d424b7a69Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-da493a8a855743cb9bf495481290dd9cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Chloro-3,5-dinitrotoluene (4.32 grams; 0.02 mole), N-ethyl-N-(2,2-diethoxyethyl)amine (3.2 grams; 0.02 mole), triethylamine (2.02 grams; 0.02 mole) and toluene (100 ml) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight resulting in the formation of a precipitate. The reaction mixture was then filtered and the filtrate washed with water, dried and stripped of solvent to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)-2,6-dinitro-p-toluidine. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture was heated at reflux overnight resulting in the formation of a precipitate The reaction mixture was then filtered the filtrate washed with water dried
Source ID: ord-b9624842cc48450d8ca1d1793312fb22Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Chloro-3,5-dinitrobenzotrifluoride (5.4 grams; 0.02 mole) dissolved in toluene (50 ml) and a solution of N-ethyl-N-(2,2-diethoxyethyl)amine (3.2 grams; 0.02 mole) and triethylamine (2.02 grams; 0.02 mole in toluene (50 ml) were charged into a glass reaction vessel equipped with stirrer, thermometer and reflux condenser. The mixture was heated at reflux overnight resulting in the formation of a precipitate. The reaction mixture was then filtered and the filtrate was washed with water, dried and stripped of solvent to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)-2,6-dinitro-4-trifluoromethylaniline. equipped with stirrer thermometer and reflux condenser The mixture was heated at reflux overnight resulting in the formation of a precipitate The reaction mixture was then filtered the filtrate was washed with water dried
Source ID: ord-e06ee16277c14ee9b483fa8182be6a7cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Ethylamine (38 grams) and 1-bromo-2,2-diethoxyethane (20 grams) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight. After this time the mixture was washed with aqueous sodium hydroxide and the organic phase separated from the aqueous phase. The organic phase was then distilled to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)amine as an oil. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture was heated at reflux overnight After this time the mixture was washed with aqueous sodium hydroxide the organic phase separated from the aqueous phase The organic phase was then distilled
Source ID: ord-8bfcf25171014b779da7e48d424b7a69PubChem References
These sources are listed in the compound's public database record.
Related Products
12 related records
CAS 69128-20-7
CAS 62773-95-9
CAS 1343344-74-0
CAS 60912-32-5
CAS 82516-06-1
CAS 1466936-47-9
CAS 98961-86-5
CAS 77738-97-7
CAS 98137-53-2
CAS 56548-04-0
CAS 110675-66-6
CAS 57366-77-5
Request a Quote
Send the required specification, quantity, destination and intended use. The CATO team will review availability and respond.