No renderable structure data available
C1=CC(=C(C=C1Cl)C(=O)NN)ClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2,5-dichlorobenzohydrazide |
|---|---|
| IUPAC Name | — |
| CAS Number | 67487-35-8 |
| Database ID | 144246 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2,5-dichlorobenzohydrazide (CAS 67487-35-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 144246
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
9 reactions · 9 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-d015d923059d446495bc4eb1e6f8d913Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-ef11e26ea0834e3c81827d31acbb2aecConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-ef11e26ea0834e3c81827d31acbb2aecConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-6b6dfbab97d24624aa2762b3813fda4cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-6b6dfbab97d24624aa2762b3813fda4cConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-d015d923059d446495bc4eb1e6f8d913Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-991ee6590b3e4ca985827a10f7758eefConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-ef11e26ea0834e3c81827d31acbb2aecConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,5-Dichlorobenzohydrazide (one equivalent) and triethylamine (one equivalent) were warmed in 500 mL of 1,2-dichloroethane until the solid material had dissolved. On cooling, 9,9-dioctyl-9H-fluorene-2-carbonyl chloride (one equivalent) was added and the mixture stirred at RT for two days. The insolubles were filtered off and the filtrate evaporated to give an oil. This was taken up in heptane and the precipitated solid filtered off. The remaining solution was dried (MgSO4) and concentrated to give the desired intermediate. had dissolved On cooling The insolubles were filtered off the filtrate evaporated to give an oil the precipitated solid filtered off The remaining solution was dried (MgSO4) concentrated
Source ID: ord-6b6dfbab97d24624aa2762b3813fda4cPubChem References
These sources are listed in the compound's public database record.
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