No renderable structure data available
C(CBr)C=OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 3-bromopropanal |
|---|---|
| IUPAC Name | — |
| CAS Number | 65032-54-4 |
| Database ID | 12465525 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
3-bromopropanal (CAS 65032-54-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 12465525
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6af1adad9f2347f1a44630bea2204fdfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1,1-Dimethylprop-2-ynylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-(1,1-dimethylprop-2-ynylamino)propionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-70bb1256102c4e6d88d910331da573d7Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1,1-Dimethylprop-2-ynylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-(1,1-dimethylprop-2-ynylamino)propionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-70bb1256102c4e6d88d910331da573d7Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: But-3-enylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-but-3-enylaminopropionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-1c2e3ad5a6b148598b64709045a818e8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: But-3-enylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-but-3-enylaminopropionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-1c2e3ad5a6b148598b64709045a818e8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1,1-Dimethylprop-2-ynylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-(1,1-dimethylprop- 2-ynylamino)propionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-a2cb8a2021234a38922dd2d600e849fcConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: But-3-enylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-but-3-enylaminopropionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-b30c86f38bec475a920a87a9daaf345fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: But-3-enylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-but-3-enylaminopropionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-b30c86f38bec475a920a87a9daaf345fConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6af1adad9f2347f1a44630bea2204fdfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1,1-Dimethylprop-2-ynylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-(1,1-dimethylprop-2-ynylamino)propionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-1a9cc3e8b4ca4ab598e33cec1144356cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: But-3-enylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-but-3-enylaminopropionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-ba3e4f0f81ac43709593fb80dc0b9189Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1,1-Dimethylprop-2-ynylamine (1.0 mole), the diethyl acetal of 3-bromopropionaldehyde (1.0 mole) and methanol (100 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux with stirring for a period of about 6 hours. After this time the reaction mixture is cooled to room temperature and sodium hydroxide (20 grams) is added. The reaction mixture is then stirred for an additional period of about 16 hours. The mixture is then filtered and the filtrate is distilled to yield the desired product the diethyl acetal of 3-(1,1-dimethylprop-2-ynylamino)propionaldehyde. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux The reaction mixture is then stirred for an additional period of about 16 hours The mixture is then filtered the filtrate is distilled
Source ID: ord-9c9763c6e4ed4d858581c593f3bcca91PubChem References
These sources are listed in the compound's public database record.
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