No renderable structure data available
C1=CC=C(C=C1)S(=O)(=O)NCCClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-(2-chloroethyl)benzenesulfonamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 6453-86-7 |
| Database ID | 4562550 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-(2-chloroethyl)benzenesulfonamide (CAS 6453-86-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 4562550
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6b33a874cedc43fa8056e09cf66dc6f3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6b33a874cedc43fa8056e09cf66dc6f3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6b33a874cedc43fa8056e09cf66dc6f3Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-af217c8a116d4497901a09f40495c96cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-af217c8a116d4497901a09f40495c96cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-bbdb7aeb229149d69989fc0654834b63Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-bbdb7aeb229149d69989fc0654834b63Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-13de535d5daa4e4f81e5d991e962055fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-07de4e76d59442e0b860f1a7492f770dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-99623e4895ef462b8314da98f44f0061Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 g. of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for 1 hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for 1 hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-bfe23ce19e7d4a41b36135fff85617d6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 40.2 of N-(β-hydroxyethyl)-benzene sulfonamide was slurried in 100 ml. of carbon tetrachloride containing 5 drops of piperidine. Then, 47.6 g. of sulfonyl chloride was added over 10 minutes, keeping the temperature at 20°-25° C. during the addition. The reaction was completed by heating on a steam bath for one hour. The mixture was concentrated on the steam bath, dissolved in benzene and washed twice with dilute aqueous solution of sodium chloride, dried over magnesium sulfate, filtered and the benzene evaporated on the steam bath with air. The product was crystallized from benzene cyclohexane to yield 28.0 g. of product, m.p. 58°-62° C. at 20°-25° C. during the addition by heating on a steam bath for one hour The mixture was concentrated on the steam bath dissolved in benzene washed twice with dilute aqueous solution of sodium chloride dried over magnesium sulfate filtered the benzene evaporated on the steam bath with air The product was crystallized from benzene cyclohexane to yield 28.0 g
Source ID: ord-985ec50cb34342228281cf693ce31418PubChem References
These sources are listed in the compound's public database record.
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