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C1C(=O)NC(=O)N1NChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 1-aminoimidazolidine-2,4-dione |
|---|---|
| IUPAC Name | — |
| CAS Number | 6301-02-6 |
| Database ID | 72823 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
1-aminoimidazolidine-2,4-dione (CAS 6301-02-6) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 72823
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-3315ee17a51445439c70da63eee95e27Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-53841e2ef5fc46d7ab287f1ea6f4ebaaConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-7a1e4a30f3c342569a2aba280257c3caConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-93c776fed3ed4e1a8e65896e7531eea3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-bb405fefd1e1488d81e94a9982bbd395Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-8616cfeb3ddf4045ac8418dc9cf8235eConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-3315ee17a51445439c70da63eee95e27Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.15 g. (0.01 mol.) of 1-amino-2,4-dioxoimidazolidine are dissolved in 50 ml. of dioxane while heating. The solution is permitted to cool to room temperature while stirring, wherein a portion of the 1-amino-2,4-dioxoimidazolidine crystallizes out. 2.05 g. (0.01 mol.) of α-isocyanatobenzeneacetic acid, ethyl ester are added and the reation mixture is stirred overnight at room temperature. On the next day the mixture is concentrated and the residue is triturated with ether. 3.0 g. of α-[[[(2,4-dioxo-1-imidazolidinyl)amino]-carbonyl] amino]benzeneacetic acid, ethyl ester are obtained, m.p. 148°-151°. wherein a portion of the 1-amino-2,4-dioxoimidazolidine crystallizes out the reation mixture is stirred overnight at room temperature On the next day the mixture is concentrated the residue is triturated with ether
Source ID: ord-5135711ffbba467f97cb00c6db5a74f4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.15 g. (0.01 mol.) of 1-amino-2,4-dioxoimidazolidine are dissolved in 50 ml. of dioxane while heating. The solution is permitted to cool to room temperature while stirring, wherein a portion of the 1-amino-2,4-dioxoimidazolidine crystallizes out. 2.05 g. (0.01 mol.) of α-isocyanatobenzeneacetic acid, ethyl ester are added and the reation mixture is stirred overnight at room temperature. On the next day the mixture is concentrated and the residue is triturated with ether. 3.0 g. of α-[[[(2,4-dioxo-1-imidazolidinyl)amino]-carbonyl] amino]benzeneacetic acid, ethyl ester are obtained, m.p. 148°-151°. wherein a portion of the 1-amino-2,4-dioxoimidazolidine crystallizes out the reation mixture is stirred overnight at room temperature On the next day the mixture is concentrated the residue is triturated with ether
Source ID: ord-5135711ffbba467f97cb00c6db5a74f4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 11.5 g. (0.1 mol.) of 1-amino-2,4-dioxoimidazolidine are thoroughly stirred into 150 ml. of absolute tetrahydrofuran. A solution of 15 g. (0.15 mol.) of phosgene in 25 ml. of absolute tetrahydrofuran is added dropwise at 0°-5° over 20 minutes. The mixture is then stirred for 3 hours at room temperature. An almost clear solution results. This is filtered and the solvent is evaporated in vacuum. The oily residue crystallizes on trituration with petroleum ether to obtain 1-(chlorocarbonylamino)-2,4-dioxoimidazolidine, yield 17.2 g., m.p. 126° (dec.). An almost clear solution results This is filtered the solvent is evaporated in vacuum The oily residue crystallizes on trituration with petroleum ether
Source ID: ord-0d12a62cec574ae484393977e3db348eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 11.5 g. (0.1 mol.) of 1-amino-2,4-dioxoimidazolidine are thoroughly stirred into 150 ml. of absolute tetrahydrofuran. A solution of 15 g. (0.15 mol.) of phosgene in 25 ml. of absolute tetrahydrofuran is added dropwise at 0°-5° over 20 minutes. The mixture is then stirred for 3 hours at room temperature. An almost clear solution results. This is filtered and the solvent is evaporated in vacuum. The oily residue crystallizes on trituration with petroleum ether to obtain 1-(chlorocarbonylamino)-2,4-dioxoimidazolidine, yield 17.2 g., m.p. 126° (dec.). An almost clear solution results This is filtered the solvent is evaporated in vacuum The oily residue crystallizes on trituration with petroleum ether
Source ID: ord-c4cc6d670166462285eaefd03e7c900bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 11.5 g. (0.1 mol.) of 1-amino-2,4-dioxoimidazolidine are thoroughly stirred into 150 ml. of absolute tetrahydrofuran. A solution of 15 g. (0.15 mol.) of phosgene in 25 ml. of absolute tetrahydrofuran is added dropwise at 0°-5° over 20 minutes. The mixture is then stirred for 3 hours at room temperature. An almost clear solution results. This is filtered and the solvent is evaporated in vacuum. The oily residue crystallizes on trituration with petroleum ether to obtain 1-(chlorocarbonylamino)-2,4-dioxoimidazolidine, yield 17.2 g., m.p. 126° (dec.). An almost clear solution results This is filtered the solvent is evaporated in vacuum The oily residue crystallizes on trituration with petroleum ether
Source ID: ord-c4cc6d670166462285eaefd03e7c900bPubChem References
These sources are listed in the compound's public database record.
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