No renderable structure data available
C1CCC(C1)CCCCOChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 4-cyclopentylbutan-1-ol |
|---|---|
| IUPAC Name | — |
| CAS Number | 5732-93-4 |
| Database ID | 21797643 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
4-cyclopentylbutan-1-ol (CAS 5732-93-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 21797643
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
11 reactions · 11 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-03542122a2ab44859cfbb39f2891307bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-cyclopentyl-butan-1-ol (3.1 g, 22 mmol) in acetonitrile (200 mL) was treated with dibromotriphenylphosphorane (10.1 g, 23.9 mmol). The reaction was stirred for two hours and quenched with water (10 mL). The reaction was diluted with dichloromethane (300 mL) and washed with water (3×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield (4-bromo-butyl)-cyclopentane as a colorless oil (3.37 g, 76%). 1H NMR (CDCl3, 300 MHz) δ 3.42 (t, 7.0 Hz, 2H), 1.9-1.7 (m, 4H), 1.6-1.3 (m, 9H), 1.07 (m, 2H). quenched with water (10 mL) The reaction was diluted with dichloromethane (300 mL) washed with water (3×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-b5f51980639f45d28710b6260d01c6beConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Cyclopentyl-butyraldehyde (4.9 g, 35 mmol) was taken up in ethanol (100 mL) and treated slowly with sodium borohydride (1.72 g, 4.54 mmol). The reaction was stirred for three days and quenched with water (10 mL). The reaction was diluted with dichloromethane (200 mL) and washed with water (2×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield 4-cyclopentyl-butan-1-ol as a colorless oil (3.12 g, 63%). quenched with water (10 mL) The reaction was diluted with dichloromethane (200 mL) washed with water (2×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-1300ab512c8a4751bb1502d043ef4969Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-cyclopentyl-butan-1-ol (3.1 g, 22 mmol) in acetonitrile (200 mL) was treated with dibromotriphenylphosphorane (10.1 g, 23.9 mmol). The reaction was stirred for two hours and quenched with water (10 mL). The reaction was diluted with dichloromethane (300 mL) and washed with water (3×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield (4-bromo-butyl)-cyclopentane as a colorless oil (3.37 g, 76%). 1H NMR (CDCl3, 300 MHz) δ 3.42 (t, 7.0 Hz, 2 H), 1.9-1.7 (m, 4 H), 1.6-1.3 (m, 9 H), 1.07 (m, 2 H). quenched with water (10 mL) The reaction was diluted with dichloromethane (300 mL) washed with water (3×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-63974033f3584ad7ab7a7ccdab11a245Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Cyclopentyl-butyraldehyde (4.9 g, 35 mmol) was taken up in ethanol (100 mL) and treated slowly with sodium borohydride (1.72 g, 4.54 mmol). The reaction was stirred for three days and quenched with water (10 mL). The reaction was diluted with dichloromethane (200 mL) and washed with water (2×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield 4-cyclopentyl-butan-1-ol as a colorless oil (3.12 g, 63%). quenched with water (10 mL) The reaction was diluted with dichloromethane (200 mL) washed with water (2×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-1612288e8b024818bf4af09b0642a0ccConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Cyclopentyl-butyraldehyde (4.9 g, 35 mmol) was taken up in ethanol (100 mL) and treated slowly with sodium borohydride (1.72 g, 4.54 mmol). The reaction was stirred for three days and quenched with water (10 mL). The reaction was diluted with dichloromethane (200 mL) and washed with water (2×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield 4-cyclopentyl-butan-1-ol as a colorless oil (3.12 g, 63%). quenched with water (10 mL) The reaction was diluted with dichloromethane (200 mL) washed with water (2×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-1612288e8b024818bf4af09b0642a0ccConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-03542122a2ab44859cfbb39f2891307bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-cyclopentyl-butan-1-ol (3.1 g, 22 mmol) in acetonitrile (200 mL) was treated with dibromotriphenylphosphorane (10.1 g, 23.9 mmol). The reaction was stirred for two hours and quenched with water (10 mL). The reaction was diluted with dichloromethane (300 mL) and washed with water (3×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield (4-bromo-butyl)-cyclopentane as a colorless oil (3.37 g, 76%). 1H NMR (CDCl3, 300 MHz) δ 3.42 (t, 7.0 Hz, 2H), 1.9-1.7 (m, 4H), 1.6-1.3 (m, 9H), 1.07 (m, 2H). quenched with water (10 mL) The reaction was diluted with dichloromethane (300 mL) washed with water (3×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-b5f51980639f45d28710b6260d01c6beConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Cyclopentyl-butyraldehyde (4.9 g, 35 mmol) was taken up in ethanol (100 mL) and treated slowly with sodium borohydride (1.72 g, 4.54 mmol). The reaction was stirred for three days and quenched with water (10 mL). The reaction was diluted with dichloromethane (200 mL) and washed with water (2×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield 4-cyclopentyl-butan-1-ol as a colorless oil (3.12 g, 63%). quenched with water (10 mL) The reaction was diluted with dichloromethane (200 mL) washed with water (2×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-1300ab512c8a4751bb1502d043ef4969Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-cyclopentyl-butan-1-ol (3.1 g, 22 mmol) in acetonitrile (200 mL) was treated with dibromotriphenylphosphorane (10.1 g, 23.9 mmol). The reaction was stirred for two hours and quenched with water (10 mL). The reaction was diluted with dichloromethane (300 mL) and washed with water (3×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield (4-bromo-butyl)-cyclopentane as a colorless oil (3.37 g, 76%). 1H NMR (CDCl3, 300 MHz) δ 3.42 (t, 7.0 Hz, 2 H), 1.9-1.7 (m, 4 H), 1.6-1.3 (m, 9 H), 1.07 (m, 2 H). quenched with water (10 mL) The reaction was diluted with dichloromethane (300 mL) washed with water (3×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-63974033f3584ad7ab7a7ccdab11a245Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Cyclopentyl-butyraldehyde (4.9 g, 35 mmol) was taken up in ethanol (100 mL) and treated slowly with sodium borohydride (1.72 g, 4.54 mmol). The reaction was stirred for three days and quenched with water (10 mL). The reaction was diluted with dichloromethane (200 mL) and washed with water (2×100 mL). The organic phase was dried (MgSO4), filtered, and concentrated to yield an oil. The product was passed through a pad of silica to yield 4-cyclopentyl-butan-1-ol as a colorless oil (3.12 g, 63%). quenched with water (10 mL) The reaction was diluted with dichloromethane (200 mL) washed with water (2×100 mL) The organic phase was dried (MgSO4) filtered concentrated to yield an oil
Source ID: ord-1612288e8b024818bf4af09b0642a0ccPubChem References
These sources are listed in the compound's public database record.
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