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BrC(C)CCCCCCChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-bromooctane |
|---|---|
| IUPAC Name | — |
| CAS Number | 557-35-7 |
| Database ID | 79046 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-bromooctane (CAS 557-35-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 79046
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-93be332aad934666a1dc113f95802664Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e940c895f84c432cbf5c9683ff10f781Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The procedure used is that of GENERAL PROCEDURE III except that 2-bromooctane is used as compound (1) in step (a), formaldehyde is used in place of ethylene oxide in step (b), y=1, and propyl bromide is used in place of methyl iodide in step (h).
Source ID: ord-0fd3d43f752f45ffbe5d4694f158d06bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium hydride (0.11 g) was added to a solution of 3-azabicyclo[3.1.0]hexane-2,4-dione (0.3 g) and 2-bromooctane (0.52 g) in dimethylformamide (5 ml) and the resulting mixture was stirred at room temperature under a nitrogen atmosphere for 48 hours. The mixture was diluted with water (15 ml) and then extracted with toluene (20 ml). The organic extract was washed with water (15 ml), dried (MgSO4) and evaporated in vacuo. The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg) to give the title compound as a colourless oil. extracted with toluene (20 ml) The organic extract was washed with water (15 ml) dried (MgSO4) evaporated in vacuo The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg)
Source ID: ord-161626737cb6480f9d6a0773d0159a65Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-93be332aad934666a1dc113f95802664Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-93be332aad934666a1dc113f95802664Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The procedure used is that of GENERAL PROCEDURE III except that 2-bromooctane is used as compound (1) in step (a), formaldehyde is used in place of ethylene oxide in step (b), y=1, and propyl bromide is used in place of methyl iodide in step (h).
Source ID: ord-f1fb8bff4a3541f6a4fb8c2ba38f0cf2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The procedure used is that of GENERAL PROCEDURE III except that 2-bromooctane is used as compound (1) in step (a), formaldehyde is used in place of ethylene oxide in step (b), y=1, and propyl bromide is used in place of methyl iodide in step (h).
Source ID: ord-f1fb8bff4a3541f6a4fb8c2ba38f0cf2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The procedure used is that of GENERAL PROCEDURE III except that 2-bromooctane is used as compound (1) in step (a), formaldehyde is used in place of ethylene oxide in step (b), y=1, and propyl bromide is used in place of methyl iodide in step (h).
Source ID: ord-0fd3d43f752f45ffbe5d4694f158d06bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium hydride (0.11 g) was added to a solution of 3-azabicyclo[3.1.0]hexane-2,4-dione (0.3 g) and 2-bromooctane (0.52 g) in dimethylformamide (5 ml) and the resulting mixture was stirred at room temperature under a nitrogen atmosphere for 48 hours. The mixture was diluted with water (15 ml) and then extracted with toluene (20 ml). The organic extract was washed with water (15 ml), dried (MgSO4) and evaporated in vacuo. The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg) to give the title compound as a colourless oil. extracted with toluene (20 ml) The organic extract was washed with water (15 ml) dried (MgSO4) evaporated in vacuo The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg)
Source ID: ord-161626737cb6480f9d6a0773d0159a65Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium hydride (0.11 g) was added to a solution of 3-azabicyclo[3.1.0]hexane-2,4-dione (0.3 g) and 2-bromooctane (0.52 g) in dimethylformamide (5 ml) and the resulting mixture was stirred at room temperature under a nitrogen atmosphere for 48 hours. The mixture was diluted with water (15 ml) and then extracted with toluene (20 ml). The organic extract was washed with water (15 ml), dried (MgSO4) and evaporated in vacuo. The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg) to give the title compound as a colourless oil. extracted with toluene (20 ml) The organic extract was washed with water (15 ml) dried (MgSO4) evaporated in vacuo The residue was purified by Kugelrohr distillation (boiling point 130-140° C. @ 0.1 mmHg)
Source ID: ord-161626737cb6480f9d6a0773d0159a65Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e940c895f84c432cbf5c9683ff10f781PubChem References
These sources are listed in the compound's public database record.
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