zinc;propanoate

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The initial temperature of the zinc oxide and propionic acid were varied, as was the time at which the high-shear blades were engaged. Vent stack temperatures approximately six inches from the top of the mixer were monitored as a measure of the rate of reaction. Each batch was prepared by charging the mixer with 77 pounds of zinc oxide followed by spraying the dry zinc oxide with 140 pounds of propionic acid at nine pounds per minute. Starting material temperatures and the time at which the high-shear mixing blades ("choppers") were engaged are summarized below in Table 1. Vent stack temperatures approximately six inches from the top of the mixer were monitored as a measure of the rate of reaction Each batch was prepared Starting material temperatures and the time at which the high-shear mixing blades ("choppers")

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In one embodiment of the present invention, anhydrous propionic acid was mixed with dry zinc oxide to yield greater than 90 percent zinc propionate. The resulting zinc propionate was a white powder, and was in a form readily utilizable for dietary supplementation. Unlike the conventional aqueous method of preparation, the product is not precipitated and then separated from solution. Moreover, no drying of the product by vacuum desiccation, spray drying or freeze drying is required, thereby saving energy costs. In comparison, using the conventional method where the zinc oxide was dissolved in an aqueous solution of propionic acid, and the solution was heated to boiling and evaporated to yield zinc propionate crystals, the yield of zinc propionate was 75.2 percent, after two crystallizations and drying under reduced pressure for 16 hours.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In one embodiment of the present invention, anhydrous propionic acid was mixed with dry zinc oxide to yield greater than 90 percent zinc propionate. The resulting zinc propionate was a white powder, and was in a form readily utilizable for dietary supplementation. Unlike the conventional aqueous method of preparation, the product is not precipitated and then separated from solution. Moreover, no drying of the product by vacuum desiccation, spray drying or freeze drying is required, thereby saving energy costs. In comparison, using the conventional method where the zinc oxide was dissolved in an aqueous solution of propionic acid, and the solution was heated to boiling and evaporated to yield zinc propionate crystals, the yield of zinc propionate was 75.2 percent, after two crystallizations and drying under reduced pressure for 16 hours.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The initial temperature of the zinc oxide and propionic acid were varied, as was the time at which the high-shear blades were engaged. Vent stack temperatures approximately six inches from the top of the mixer were monitored as a measure of the rate of reaction. Each batch was prepared by charging the mixer with 77 pounds of zinc oxide followed by spraying the dry zinc oxide with 140 pounds of propionic acid at nine pounds per minute. Starting material temperatures and the time at which the high-shear mixing blades ("choppers") were engaged are summarized below in Table 1. Vent stack temperatures approximately six inches from the top of the mixer were monitored as a measure of the rate of reaction Each batch was prepared Starting material temperatures and the time at which the high-shear mixing blades ("choppers")

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In one embodiment of the present invention, anhydrous propionic acid was mixed with dry zinc oxide to yield greater than 90 percent zinc propionate. The resulting zinc propionate was a white powder, and was in a form readily utilizable for dietary supplementation. Unlike the conventional aqueous method of preparation, the product is not precipitated and then separated from solution. Moreover, no drying of the product by vacuum desiccation, spray drying or freeze drying is required, thereby saving energy costs. In comparison, using the conventional method where the zinc oxide was dissolved in an aqueous solution of propionic acid, and the solution was heated to boiling and evaporated to yield zinc propionate crystals, the yield of zinc propionate was 75.2 percent, after two crystallizations and drying under reduced pressure for 16 hours.