Reaction #3234693
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07151155B2
Conditions: temp:60.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The formulation used for the copolymer is given in Table 2 below. The copolymer was prepared according to the method of Example 1, except that the weight ratio of caprolactone to 1,3-dioxepane was 3 and the reaction temperature was 50° C. The carbodiimide used was Stabaxol P. After removal of the unreacted 1,3-dioxepane, the copolymer was heated to 60° C. and filtered through cheese cloth to remove agglomerated particles resulting from silica gel in the Stabaxol P. The copolymer was prepared was 50° C After removal of the unreacted 1,3-dioxepane filtered through cheese cloth to remove resulting from silica gel in the Stabaxol P
Source ID: ord-8291ca8002db48ab8da9680efa366396