No renderable structure data available
C=CCNS(=O)(=O)C1=CC=CC=C1Chemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-prop-2-enylbenzenesulfonamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 50487-70-2 |
| Database ID | 257467 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-prop-2-enylbenzenesulfonamide (CAS 50487-70-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 257467
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
8 reactions · 8 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-1f7e696c201049c5834a1c618279d3d4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-e34992c041d64e4f88ecfe12dc444722Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-e34992c041d64e4f88ecfe12dc444722Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-1f7e696c201049c5834a1c618279d3d4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
Source ID: ord-e34992c041d64e4f88ecfe12dc444722PubChem References
These sources are listed in the compound's public database record.
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