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CCC(C)NCC1=CC=C(C=C1)ClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-[(4-chlorophenyl)methyl]butan-2-amine |
|---|---|
| IUPAC Name | — |
| CAS Number | 46234-40-6 |
| Database ID | 4717029 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-[(4-chlorophenyl)methyl]butan-2-amine (CAS 46234-40-6) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 4717029
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-a43f29de73e74e5fb197c47e5e04de27Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-00b7726e4dfb4625b7f07f23a2d77e39Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of N-(4-chlorobenzyl)-N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 14 g of phenyl isothiocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 30 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylthiourea were obtained. Yield: 91%. Melting point: 134°-134.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-8fee94989e1f483d8687b053b84066ccConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of N-(4-chlorobenzyl)-N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 14 g of phenyl isothiocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 30 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylthiourea were obtained. Yield: 91%. Melting point: 134°-134.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-8fee94989e1f483d8687b053b84066ccConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 30 g (0.15 mole) of N-(4-chlorobenzyl)N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 18 g (0.15 mole) of phenyl isocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 44 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylurea were obtained. Yield: 93%. Melting point: 80°-81.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-3b5ad136fafb44e4b42c8437085d5c4aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 30 g (0.15 mole) of N-(4-chlorobenzyl)N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 18 g (0.15 mole) of phenyl isocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 44 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylurea were obtained. Yield: 93%. Melting point: 80°-81.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-3b5ad136fafb44e4b42c8437085d5c4aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of N-(4-chlorobenzyl)-N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 14 g of phenyl isothiocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 30 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylthiourea were obtained. Yield: 91%. Melting point: 134°-134.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-8fee94989e1f483d8687b053b84066ccConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-a43f29de73e74e5fb197c47e5e04de27Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-00b7726e4dfb4625b7f07f23a2d77e39Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 30 g (0.15 mole) of N-(4-chlorobenzyl)N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 18 g (0.15 mole) of phenyl isocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 44 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylurea were obtained. Yield: 93%. Melting point: 80°-81.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-3b5ad136fafb44e4b42c8437085d5c4aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of N-(4-chlorobenzyl)-N-sec.-butylamine were dissolved in 500 ml of ether. To the resulting solution, a solution of 14 g of phenyl isothiocyanate in 50 ml of ether was added dropwise, under cooling and stirring. After the dropwise addition, the temperature of the solution was gradually raised, and the solution was then stirred at room temperature for about 10 hours. The crystals which had been formed were separated by filtration. After recrystallization with a solvent mixture of hexane and ethyl alcohol, 30 g of N-(4-chlorobenzyl)-N-sec.-butyl-N'-phenylthiourea were obtained. Yield: 91%. Melting point: 134°-134.5° C. under cooling After the dropwise addition the temperature of the solution was gradually raised the solution was then stirred at room temperature for about 10 hours The crystals which had been formed were separated by filtration After recrystallization with a solvent mixture of hexane and ethyl alcohol
Source ID: ord-8fee94989e1f483d8687b053b84066ccConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-00b7726e4dfb4625b7f07f23a2d77e39PubChem References
These sources are listed in the compound's public database record.
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