No renderable structure data available
CC(C)(C)NC(=O)C1=CC(=CC=C1)BrChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 3-bromo-N-tert-butylbenzamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 42498-39-5 |
| Database ID | 603211 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
3-bromo-N-tert-butylbenzamide (CAS 42498-39-5) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 603211
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
10 reactions · 10 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-47d6c368f75045eb958f98d562371a0cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-fe8b9146f04c4760b83e4a86d2df9faeConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-d782f58911c5426093582a1a5e849716Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-5d1e6cbf2a7b481bb2e3250b5c55136eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-5d1e6cbf2a7b481bb2e3250b5c55136eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-50badff3aec54d5883dd3fe29bf6ab53Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-8f6dd870cf754a6ea8895f95441b8e3eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-fe8b9146f04c4760b83e4a86d2df9faeConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-d782f58911c5426093582a1a5e849716Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 3-bromo-benzoyl chloride (0.83 g, 3.8 mmol) in DCM (10 mL) was chilled to zero degrees and treated with tert-butylamine (1.2 mL, 11.3 mmol). Reaction was allowed to come to room temperature and stir for 4 h. Mixture was then poured onto water and washed once. Organic phase then washed with brine, dried over sodium sulfate, filtered and evaporated to amber oil (0.9 g, 94%). Reaction to come to room temperature Mixture was then poured onto water washed once Organic phase then washed with brine dried over sodium sulfate filtered evaporated to amber oil (0.9 g, 94%)
Source ID: ord-5d1e6cbf2a7b481bb2e3250b5c55136ePubChem References
These sources are listed in the compound's public database record.
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