No renderable structure data available
C1=CC=C(C=C1)SC2=C(C=C(C=C2)Cl)NChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 5-chloro-2-phenylsulfanylaniline |
|---|---|
| IUPAC Name | — |
| CAS Number | 4235-20-5 |
| Database ID | 2063717 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
5-chloro-2-phenylsulfanylaniline (CAS 4235-20-5) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 2063717
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-73aa4050f4d0480b86dfdb82eed615bcConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: An ethanol solution of 1.0 g (4.2 mmol) of 4-chloro-2-nitro-1-(phenylthio)benzene (32), prepared in the manner described above in Example 32, is shaken in a Parr hydrogenator at 30 psi hydrogen with Raney nickel at room temperature for 3 hours. The catalyst is filtered from the reaction, and the solution is concentrated under vacuum. The catalyst is filtered from the reaction the solution is concentrated under vacuum
Source ID: ord-06d48501cc78407ba0aa691f89340381Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: An ethanol solution of 1.0 g (4.2 mmol) of 4-chloro-2-nitro-1-(phenylthio)benzene (32), prepared in the manner described above in Example 32, is shaken in a Parr hydrogenator at 30 psi hydrogen with Raney nickel at room temperature for 3 hours. The catalyst is filtered from the reaction, and the solution is concentrated under vacuum. The catalyst is filtered from the reaction the solution is concentrated under vacuum
Source ID: ord-06d48501cc78407ba0aa691f89340381Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: An ethanol solution of 1.0 g (4.2 mmol) of 4-chloro-2-nitro-1-(phenylthio)benzene (32), prepared in the manner described above in Example 32, is shaken in a Parr hydrogenator at 30 psi hydrogen with Raney nickel at room temperature for 3 hours. The catalyst is filtered from the reaction, and the solution is concentrated under vacuum. The catalyst is filtered from the reaction the solution is concentrated under vacuum
Source ID: ord-06d48501cc78407ba0aa691f89340381Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: An ethanol solution of 1.0 g (4.2 mmol) of 4-chloro-2-nitro-1-(phenylthio)benzene (32), prepared in the manner described above in Example 32, is shaken in a Parr hydrogenator at 30 psi hydrogen with Raney nickel at room temperature for 3 hours. The catalyst is filtered from the reaction, and the solution is concentrated under vacuum. The catalyst is filtered from the reaction the solution is concentrated under vacuum
Source ID: ord-06d48501cc78407ba0aa691f89340381Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-73aa4050f4d0480b86dfdb82eed615bcConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro-1-(phenylthio)benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-cdf47578dafe4651a43501bc9198d941Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro-1-(phenylthio)-benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-31158638391a4c08a72a04dd78da65b2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro-1-(phenylthio)-benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-31158638391a4c08a72a04dd78da65b2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro-1-(phenylthio)-benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-31158638391a4c08a72a04dd78da65b2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro1-(phenylthio)benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-402d9e4779ac498c84e383704c5630cfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 4-chloro-2-nitro-1-(phenylthio)benzene (11.0 g) and Raney nickel in ethanol (3A; 9.3 mL) was reacted in a Parr Hydrogenator under hydrogen atmosphere at 5 psi and room temperature. When the theoretical amount of hydrogen uptake was reached, the reaction was filtered to remove the catalyst and evaporated in vacuo to yield 8.61 g (88%) of a light orange solid. mp: 59°-61° C. the reaction was filtered to remove the catalyst evaporated in vacuo
Source ID: ord-b49276390ca141b492c5cc8b3720da99PubChem References
These sources are listed in the compound's public database record.
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