1,1-diethoxydecane

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Decanal diethyl acetal was prepared by reacting 316 g decanal with 354 g triethyl orthoformate in the presence of 7.6 g ammonium nitrate dissolved in 20 ml. ethanol at a temperature of 50° C. for a period of time of 4 hours. The resulting product was quenched with 32 g sodium methoxide and distilled at 170° C. at 8.0 mm Hg pressure. Then, into a 2 liter reaction flask equipped with stirrer, thermometer, heating mantle, addition funnel, vacuum apparatus, and reflux condenser the following ingredients are added at 20°: dissolved in 20 ml The resulting product was quenched with 32 g sodium methoxide distilled at 170° C. at 8.0 mm Hg pressure Then, into a 2 liter reaction flask equipped with stirrer thermometer, heating mantle, addition funnel, vacuum apparatus reflux condenser the following ingredients are added at 20°

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Decanal diethyl acetal was prepared by reacting 316 g decanal with 354 g triethyl orthoformate in the presence of 7.6 g ammonium nitrate dissolved in 20 ml. ethanol at a temperature of 50° C. for a period of time of 4 hours. The resulting product was quenched with 32 g sodium methoxide and distilled at 170° C. at 8.0 mm Hg pressure. Then, into a 2 liter reaction flask equipped with stirrer, thermometer, heating mantle, addition funnel, vacuum apparatus, and reflux condenser the following ingredients are added at 20°: dissolved in 20 ml The resulting product was quenched with 32 g sodium methoxide distilled at 170° C. at 8.0 mm Hg pressure Then, into a 2 liter reaction flask equipped with stirrer thermometer, heating mantle, addition funnel, vacuum apparatus reflux condenser the following ingredients are added at 20°

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Decanal diethyl acetal was prepared by reacting 316 g decanal with 354 g triethyl orthoformate in the presence of 7.6 g ammonium nitrate dissolved in 20 ml. ethanol at a temperature of 50° C. for a period of time of 4 hours. The resulting product was quenched with 32 g sodium methoxide and distilled at 170° C. at 8.0 mm Hg pressure. Then, into a 2 liter reaction flask equipped with stirrer, thermometer, heating mantle, addition funnel, vacuum apparatus, and reflux condenser the following ingredients are added at 20°: dissolved in 20 ml The resulting product was quenched with 32 g sodium methoxide distilled at 170° C. at 8.0 mm Hg pressure Then, into a 2 liter reaction flask equipped with stirrer thermometer, heating mantle, addition funnel, vacuum apparatus reflux condenser the following ingredients are added at 20°