No renderable structure data available
CC1=C(C(=CC=C1)C)CCOChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-(2,6-dimethylphenyl)ethanol |
|---|---|
| IUPAC Name | — |
| CAS Number | 30595-80-3 |
| Database ID | 33942 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-(2,6-dimethylphenyl)ethanol (CAS 30595-80-3) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 33942
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-57e2a27f9b684d53a940384487144d48Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-1d30dff30bc74c148be6fa80ccee5c6aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzeneethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THP (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colorless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-fe655ffd60714605834c69fba92aec09Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzeneethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THP (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colorless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-fe655ffd60714605834c69fba92aec09Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-b45e9f33fcc441fbb18d0d192db745b3Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution f 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-acc0d0ac996740c1aa636be541a52c57Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution f 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-acc0d0ac996740c1aa636be541a52c57Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-0676b7bfc0cc48debb75b2eb79897d29Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-1d30dff30bc74c148be6fa80ccee5c6aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzeneethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THP (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colorless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-fe655ffd60714605834c69fba92aec09Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution of 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110°-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-b45e9f33fcc441fbb18d0d192db745b3Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: NaH (46% dispersion in oil; 4.2 g) was added portionwise to a solution f 2,6-dimethylbenzenethanol (6.0 g) and 1,6-dibromohexane (19.52 g) in THF (50 ml) under nitrogen. The mixture was refluxed for 18 h and treated cautiously with H2O (20 ml). The resulting emulsion was extracted with ER (3×100 ml) and the dried extract was evaporated to leave a yellow oil. Excess 1,6-dibromohexane was removed under reduced pressure and the residue was purified on a column of silica (300 ml) [B] to give the title compound as a colourless oil (6.6 g) b.p. 110-115°/0.4 mmHg. The mixture was refluxed for 18 h The resulting emulsion was extracted with ER (3×100 ml) the dried extract was evaporated to leave a yellow oil Excess 1,6-dibromohexane was removed under reduced pressure the residue was purified on a column of silica (300 ml) [B]
Source ID: ord-acc0d0ac996740c1aa636be541a52c57PubChem References
These sources are listed in the compound's public database record.
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