No renderable structure data available
CCCC(=O)C1=C(C=C(C=C1C)C)CChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 1-(2,4,6-trimethylphenyl)butan-1-one |
|---|---|
| IUPAC Name | — |
| CAS Number | 29786-97-8 |
| Database ID | 251160 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
1-(2,4,6-trimethylphenyl)butan-1-one (CAS 29786-97-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 251160
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
11 reactions · 11 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-8373cd21ee0f4561a23fa8ef645b3302Conditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2′,4′,6′-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction zmixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without farther purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-70311de3fa71442e940a26947180f5bfConditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres) was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2',4',6'-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction mixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without further purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-69734882ed034e54a02ab73a63810091Conditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2′,4′,6′-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction zmixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without farther purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-70311de3fa71442e940a26947180f5bfConditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2′,4′,6′-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction zmixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without farther purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-70311de3fa71442e940a26947180f5bfConditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres) was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2',4',6'-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction mixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without further purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-69734882ed034e54a02ab73a63810091Conditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres) was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2',4',6'-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction mixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without further purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-69734882ed034e54a02ab73a63810091Conditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2′,4′,6′-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction zmixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without farther purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-70311de3fa71442e940a26947180f5bfConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-8373cd21ee0f4561a23fa8ef645b3302Conditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres ) was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2',4',6'-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction mixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without further purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-293e85f8c8d64c548a51c90d4477fd4dConditions: temp:50.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium (1.0 g, 42.1 mmol, spheres) was cautiously added to 25 mL of absolute EtOH with stirring. After the sodium had dissolved, diethyl oxalate (6.0 g, 42.1 mmol) was added dropwise to the resulting solution at 0° C., followed by addition of a solution of 2',4',6'-trimethylbutyrophenone (8 g, 42.1 mmol) in 5 mL of absolute EtOH. The reaction mixture was slowly warmed to 50° C. and stirred overnight. The solvent was then evaporated. The resulting residue was washed with hexane, diluted with water, acidified with 1 N HCl, and then extracted with ether. The extracts were washed with brine, dried over Na2SO4 and concentrated to give 6.5 g of an oil which was used in the next reaction without further purification. stirred overnight The solvent was then evaporated The resulting residue was washed with hexane diluted with water extracted with ether The extracts were washed with brine dried over Na2SO4 concentrated
Source ID: ord-69734882ed034e54a02ab73a63810091PubChem References
These sources are listed in the compound's public database record.
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