No renderable structure data available
C1=C(C=C(C(=C1Br)N)Br)NChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2,6-dibromobenzene-1,4-diamine |
|---|---|
| IUPAC Name | — |
| CAS Number | 29213-03-4 |
| Database ID | 653341 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2,6-dibromobenzene-1,4-diamine (CAS 29213-03-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 653341
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
10 reactions · 10 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-9e94aa6d241c420e876245eab108f579Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of 2,6-Dibromo-4-nitroaniline are taken up in 250 ml of ethanol, 250 ml of ethyl acetate, 100 ml of dimethylformamide and 90 ml of methylene chloride and, after addition of 3.3 g of 5% moist platinum/active carbon catalyst, hydrogenated at room temperature under 50 psi for one hour. The solvent is then distilled off in a rotary evaporator, and the residue is triturated with diethyl ether, filtered off with suction and washed several times with petroleum ether. The solvent is then distilled off in a rotary evaporator the residue is triturated with diethyl ether filtered off with suction washed several times with petroleum ether
Source ID: ord-0ad8c440815246b7b935f8ec8b1a95bfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 3.0 g of 2,6-dibromo-4-nitro-aniline are dissolved in 150 ml of ethanol, 150 ml of ethyl acetate and 30 ml of dimethylformamide and, after addition of 0.5 g of platinum-on-charcoal (5%), are hydrogenated in a Parr apparatus at room temperature under a hydrogen pressure of 1.5 bar for 1 hour. After cooling, the mixture is filtered, the solvent is distilled off in a rotary evaporator and the residue is purified by column chromatography. are hydrogenated in a Parr apparatus at room temperature under a hydrogen for 1 hour After cooling the mixture is filtered the solvent is distilled off in a rotary evaporator the residue is purified by column chromatography
Source ID: ord-8b2f955d9d184db98e857024beb0a8d0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 3.0 g of 2,6-dibromo-4-nitro-aniline are dissolved in 150 ml of ethanol, 150 ml of ethyl acetate and 30 ml of dimethylformamide and, after addition of 0.5 g of platinum-on-charcoal (5%), are hydrogenated in a Parr apparatus at room temperature under a hydrogen pressure of 1.5 bar for 1 hour. After cooling, the mixture is filtered, the solvent is distilled off in a rotary evaporator and the residue is purified by column chromatography. are hydrogenated in a Parr apparatus at room temperature under a hydrogen for 1 hour After cooling the mixture is filtered the solvent is distilled off in a rotary evaporator the residue is purified by column chromatography
Source ID: ord-8b2f955d9d184db98e857024beb0a8d0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of 2,6-Dibromo-4-nitroaniline are taken up in 250 ml of ethanol, 250 ml of ethyl acetate, 100 ml of dimethylformamide and 90 ml of methylene chloride and, after addition of 3.3 g of 5% moist platinum/active carbon catalyst, hydrogenated at room temperature under 50 psi for one hour. The solvent is then distilled off in a rotary evaporator, and the residue is triturated with diethyl ether, filtered off with suction and washed several times with petroleum ether. The solvent is then distilled off in a rotary evaporator the residue is triturated with diethyl ether filtered off with suction washed several times with petroleum ether
Source ID: ord-0ad8c440815246b7b935f8ec8b1a95bfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of 2,6-Dibromo-4-nitroaniline are taken up in 250 ml of ethanol, 250 ml of ethyl acetate, 100 ml of dimethylformamide and 90 ml of methylene chloride and, after addition of 3.3 g of 5% moist platinum/active carbon catalyst, hydrogenated at room temperature under 50 psi for one hour. The solvent is then distilled off in a rotary evaporator, and the residue is triturated with diethyl ether, filtered off with suction and washed several times with petroleum ether. The solvent is then distilled off in a rotary evaporator the residue is triturated with diethyl ether filtered off with suction washed several times with petroleum ether
Source ID: ord-0ad8c440815246b7b935f8ec8b1a95bfConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-9e94aa6d241c420e876245eab108f579Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 3.0 g of 2,6-dibromo-4-nitroaniline are dissolved in 150 ml of ethanol, 150 ml of ethyl acetate and 30 ml of dimethylformamide and, after addition of 0.5 g of platinum on carbon (5%), hydrogenated under a pressure of 1.5 bar of hydrogen in a Parr apparatus at room temperature for 1 hour. Cooling is followed by filtration, the solvent is distilled off in a rotary evaporator, and the residue is purified by column chromatography. Cooling is followed by filtration the solvent is distilled off in a rotary evaporator the residue is purified by column chromatography
Source ID: ord-b1ee345baeaf4d92a55db75fab27a8a9Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 3.0 g of 2,6-dibromo-4-nitro-aniline are dissolved in 150 ml of ethanol, 150 ml of ethyl acetate and 30 ml of dimethylformamide and, after addition of 0.5 g of platinum-on-charcoal (5%), are hydrogenated in a Parr apparatus at room temperature under a hydrogen pressure of 1.5 bar for 1 hour. After cooling, the mixture is filtered, the solvent is distilled off in a rotary evaporator and the residue is purified by column chromatography. are hydrogenated in a Parr apparatus at room temperature under a hydrogen for 1 hour After cooling the mixture is filtered the solvent is distilled off in a rotary evaporator the residue is purified by column chromatography
Source ID: ord-8b2f955d9d184db98e857024beb0a8d0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 20 g of 2,6-Dibromo-4-nitroaniline are taken up in 250 ml of ethanol, 250 ml of ethyl acetate, 100 ml of dimethylformamide and 90 ml of methylene chloride and, after addition of 3.3 g of 5% moist platinum/active carbon catalyst, hydrogenated at room temperature under 50 psi for one hour. The solvent is then distilled off in a rotary evaporator, and the residue is triturated with diethyl ether, filtered off with suction and washed several times with petroleum ether. The solvent is then distilled off in a rotary evaporator the residue is triturated with diethyl ether filtered off with suction washed several times with petroleum ether
Source ID: ord-0ad8c440815246b7b935f8ec8b1a95bfPubChem References
These sources are listed in the compound's public database record.
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