No renderable structure data available
C1=COC(=C1)CC#NChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-(furan-2-yl)acetonitrile |
|---|---|
| IUPAC Name | — |
| CAS Number | 2745-25-7 |
| Database ID | 10909515 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-(furan-2-yl)acetonitrile (CAS 2745-25-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 10909515
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b370ff34a1aa497d9791e5db90ce9bb3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-5559f03edafa4287b541eef903f7fa40Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR. was refluxed for 1 hour cooled extraction with ether This solution was extracted with ether the organic phase was dried over MgSO4 evaporated under vacuum
Source ID: ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-(Furan-2-yl)acetonitrile was suspended in 300 mL of distilled water, mixed with 50 g (0.89 mmol) of potassium hydroxide and heated for 4 hours under reflux. After completion of the reaction, the reaction solution was diluted with diethyl ether and separated. The resulting aqueous layer was acidified with concentrated hydrochloric acid and extracted with ethyl acetate. The organic layer was washed with saturated aqueous sodium chloride, dried over anhydrous magnesium sulfate and filterd, and the filtrate was concentrated under reduced pressure to give 25.2 g of the desired product. heated for 4 hours under reflux After completion of the reaction separated extracted with ethyl acetate The organic layer was washed with saturated aqueous sodium chloride dried over anhydrous magnesium sulfate and filterd the filtrate was concentrated under reduced pressure
Source ID: ord-8ad6f5e198e443a5a0b4fe2b8f1ab697Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-(Furan-2-yl)acetonitrile was suspended in 300 mL of distilled water, mixed with 50 g (0.89 mmol) of potassium hydroxide and heated for 4 hours under reflux. After completion of the reaction, the reaction solution was diluted with diethyl ether and separated. The resulting aqueous layer was acidified with concentrated hydrochloric acid and extracted with ethyl acetate. The organic layer was washed with saturated aqueous sodium chloride, dried over anhydrous magnesium sulfate and filterd, and the filtrate was concentrated under reduced pressure to give 25.2 g of the desired product. heated for 4 hours under reflux After completion of the reaction separated extracted with ethyl acetate The organic layer was washed with saturated aqueous sodium chloride dried over anhydrous magnesium sulfate and filterd the filtrate was concentrated under reduced pressure
Source ID: ord-8ad6f5e198e443a5a0b4fe2b8f1ab697Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR. was refluxed for 1 hour cooled extraction with ether This solution was extracted with ether the organic phase was dried over MgSO4 evaporated under vacuum
Source ID: ord-e04ded5e86414da0b6241c4fcbfbb6f8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR. was refluxed for 1 hour cooled extraction with ether This solution was extracted with ether the organic phase was dried over MgSO4 evaporated under vacuum
Source ID: ord-e04ded5e86414da0b6241c4fcbfbb6f8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR. was refluxed for 1 hour cooled extraction with ether This solution was extracted with ether the organic phase was dried over MgSO4 evaporated under vacuum
Source ID: ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR. was refluxed for 1 hour cooled extraction with ether This solution was extracted with ether the organic phase was dried over MgSO4 evaporated under vacuum
Source ID: ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-(Furan-2-yl)acetonitrile was suspended in 300 mL of distilled water, mixed with 50 g (0.89 mmol) of potassium hydroxide and heated for 4 hours under reflux. After completion of the reaction, the reaction solution was diluted with diethyl ether and separated. The resulting aqueous layer was acidified with concentrated hydrochloric acid and extracted with ethyl acetate. The organic layer was washed with saturated aqueous sodium chloride, dried over anhydrous magnesium sulfate and filterd, and the filtrate was concentrated under reduced pressure to give 25.2 g of the desired product. heated for 4 hours under reflux After completion of the reaction separated extracted with ethyl acetate The organic layer was washed with saturated aqueous sodium chloride dried over anhydrous magnesium sulfate and filterd the filtrate was concentrated under reduced pressure
Source ID: ord-8ad6f5e198e443a5a0b4fe2b8f1ab697Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b370ff34a1aa497d9791e5db90ce9bb3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-5559f03edafa4287b541eef903f7fa40PubChem References
These sources are listed in the compound's public database record.
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