No renderable structure data available
CCCCCCCCCCCCCCN1CCOCC1Chemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 4-tetradecylmorpholine |
|---|---|
| IUPAC Name | — |
| CAS Number | 25727-93-9 |
| Database ID | 117616 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
4-tetradecylmorpholine (CAS 25727-93-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 117616
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
7 reactions · 7 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-5c4b5056adaf4f86b31e7335c89f9a6aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: In a 250-mL round bottom flask, equipped with a magnetic stirrer, a heating mantle and reflux condenser, were placed 1-bromotetradecane (15.9 g, 57.3 mmol), acetonitrile (75 mL), and morpholine (10 g, 114.7 mmol). The reaction mixture was refluxed for 4 hrs. The reaction mixture was cooled to room temperature and was concentrated to a residue on a rotary evaporator. Water and ethyl acetate were added. The organic phase was separated and washed with saturated sodium chloride solution, and then dried over anhydrous magnesium sulfate. After filtration, the solvent was evaporated to dryness affording 15.2 g (94% yield) of 4-tetradecylmorpholine as a tan oil. This intermediate was subjected to the next step without further purification. In a 250-mL round bottom flask, equipped with a magnetic stirrer a heating mantle and reflux condenser The reaction mixture was refluxed for 4 hrs was concentrated to a residue on a rotary evaporator Water and ethyl acetate were added The organic phase was separated washed with saturated sodium chloride solution dried over anhydrous magnesium sulfate After filtration the solvent was evaporated to dryness
Source ID: ord-4915d56f036b428187c79fe574ec5742Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: In a 250-mL round bottom flask, equipped with a magnetic stirrer, a heating mantle and reflux condenser, were placed 1-bromotetradecane (15.9 g, 57.3 mmol), acetonitrile (75 mL), and morpholine (10 g, 114.7 mmol). The reaction mixture was refluxed for 4 hrs. The reaction mixture was cooled to room temperature and was concentrated to a residue on a rotary evaporator. Water and ethyl acetate were added. The organic phase was separated and washed with saturated sodium chloride solution, and then dried over anhydrous magnesium sulfate. After filtration, the solvent was evaporated to dryness affording 15.2 g (94% yield) of 4-tetradecylmorpholine as a tan oil. This intermediate was subjected to the next step without further purification. In a 250-mL round bottom flask, equipped with a magnetic stirrer a heating mantle and reflux condenser The reaction mixture was refluxed for 4 hrs was concentrated to a residue on a rotary evaporator Water and ethyl acetate were added The organic phase was separated washed with saturated sodium chloride solution dried over anhydrous magnesium sulfate After filtration the solvent was evaporated to dryness
Source ID: ord-4915d56f036b428187c79fe574ec5742Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: In a 250-mL round bottom flask, equipped with a magnetic stirrer, a heating mantle and reflux condenser, were placed 1-bromotetradecane (15.9 g, 57.3 mmol), acetonitrile (75 mL), and morpholine (10 g, 114.7 mmol). The reaction mixture was refluxed for 4 hrs. The reaction mixture was cooled to room temperature and was concentrated to a residue on a rotary evaporator. Water and ethyl acetate were added. The organic phase was separated and washed with saturated sodium chloride solution, and then dried over anhydrous magnesium sulfate. After filtration, the solvent was evaporated to dryness affording 15.2 g (94% yield) of 4-tetradecylmorpholine as a tan oil. This intermediate was subjected to the next step without further purification. In a 250-mL round bottom flask, equipped with a magnetic stirrer a heating mantle and reflux condenser The reaction mixture was refluxed for 4 hrs was concentrated to a residue on a rotary evaporator Water and ethyl acetate were added The organic phase was separated washed with saturated sodium chloride solution dried over anhydrous magnesium sulfate After filtration the solvent was evaporated to dryness
Source ID: ord-4915d56f036b428187c79fe574ec5742Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-5c4b5056adaf4f86b31e7335c89f9a6aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: In a 250-mL round bottom flask, equipped with a magnetic stirrer, a heating mantle and reflux condenser, were placed 1-bromotetradecane (15.9 g, 57.3 mmol), acetonitrile (75 mL), and morpholine (10 g, 114.7 mmol). The reaction mixture was refluxed for 4 hrs. The reaction mixture was cooled to room temperature and was concentrated to a residue on a rotary evaporator. Water and ethyl acetate were added. The organic phase was separated and washed with saturated sodium chloride solution, and then dried over anhydrous magnesium sulfate. After filtration, the solvent was evaporated to dryness affording 15.2 g (94% yield) of 4-tetradecylmorpholine as a tan oil. This intermediate was subjected to the next step without further purification. In a 250-mL round bottom flask, equipped with a magnetic stirrer a heating mantle and reflux condenser The reaction mixture was refluxed for 4 hrs was concentrated to a residue on a rotary evaporator Water and ethyl acetate were added The organic phase was separated washed with saturated sodium chloride solution dried over anhydrous magnesium sulfate After filtration the solvent was evaporated to dryness
Source ID: ord-6e9b304c6ccb4b4ca1bc9fb593431ef2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: In a 250-mL round bottom flask, equipped with a magnetic stirrer, a heating mantle and reflux condenser, were placed 1-bromotetradecane (15.9 g, 57.3 mmol), acetonitrile (75 mL), and morpholine (10 g, 114.7 mmol). The reaction mixture was refluxed for 4 hrs. The reaction mixture was cooled to room temperature and was concentrated to a residue on a rotary evaporator. Water and ethyl acetate were added. The organic phase was separated and washed with saturated sodium chloride solution, and then dried over anhydrous magnesium sulfate. After filtration, the solvent was evaporated to dryness affording 15.2 g (94% yield) of 4-tetradecylmorpholine as a tan oil. This intermediate was subjected to the next step without further purification. In a 250-mL round bottom flask, equipped with a magnetic stirrer a heating mantle and reflux condenser The reaction mixture was refluxed for 4 hrs was concentrated to a residue on a rotary evaporator Water and ethyl acetate were added The organic phase was separated washed with saturated sodium chloride solution dried over anhydrous magnesium sulfate After filtration the solvent was evaporated to dryness
Source ID: ord-4915d56f036b428187c79fe574ec5742PubChem References
These sources are listed in the compound's public database record.
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