No renderable structure data available
CCS(=O)(=O)CCCNChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 3-ethylsulfonylpropan-1-amine |
|---|---|
| IUPAC Name | — |
| CAS Number | 173336-36-2 |
| Database ID | 21458690 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
3-ethylsulfonylpropan-1-amine (CAS 173336-36-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 21458690
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6d2695f384be4afbaf95779a6ae509d5Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-dc1d1443f2df4740a9d2f0f122571b10Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-dc1d1443f2df4740a9d2f0f122571b10Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3 x 150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80: 15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80: 15:5)=0.15. the mixture is extracted with 3 x 150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80: 15:5)
Source ID: ord-b5ff3cba17854961b06a91882ecffcaeConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3 x 150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80: 15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80: 15:5)=0.15. the mixture is extracted with 3 x 150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80: 15:5)
Source ID: ord-b5ff3cba17854961b06a91882ecffcaeConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-95df6171f5b845108f1c57b769b42347Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-dc1d1443f2df4740a9d2f0f122571b10Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6d2695f384be4afbaf95779a6ae509d5Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-d548dca7793b43298ff6c3f0b25544bfConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-d548dca7793b43298ff6c3f0b25544bfConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-d548dca7793b43298ff6c3f0b25544bfConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 1.0 g of 3-aminopropyl-ethyl sulfide is placed in 35 ml of methanol at 0° C.; 15.5 g of oxone in 35 ml of water are added and the mixture is stirred at 0° C. for 4 hours. 200 ml of water are added and the mixture is extracted with 3×150 ml of dichloromethane. The organic extracts are concentrated by evaporation and purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5). The title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.15. the mixture is extracted with 3×150 ml of dichloromethane The organic extracts are concentrated by evaporation purified by FC (10 g of silica gel, ethyl acetate/methanol/conc. ammonia=80:15:5)
Source ID: ord-cb5dd9e8b4b344658fe7d22437b6ddd9PubChem References
These sources are listed in the compound's public database record.
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