No renderable structure data available
CN(C)CC1=CC=C(C=C1)ClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 1-(4-chlorophenyl)-N,N-dimethylmethanamine |
|---|---|
| IUPAC Name | — |
| CAS Number | 15184-98-2 |
| Database ID | 11286707 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
1-(4-chlorophenyl)-N,N-dimethylmethanamine (CAS 15184-98-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 11286707
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-462ef7d1e76c4a9285988e89a2465fabConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-933886a7cde34b8c9ce40ea5b26c8613Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-933886a7cde34b8c9ce40ea5b26c8613Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-03212b35737c4e14a443ff8343bdb784Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-b63533599eb84943b04aa3ce51c79383Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-933886a7cde34b8c9ce40ea5b26c8613Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-462ef7d1e76c4a9285988e89a2465fabConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-3f12faea30ed496aa9c6f6843f27449dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml of tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-3f12faea30ed496aa9c6f6843f27449dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-948cee2019594fbb9465a3c6ec4ec511Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-948cee2019594fbb9465a3c6ec4ec511Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: The solution of 141 g of α,p-dichlorotoluene in 200 ml tetrahydrofuran is added dropwise to an ice-cold saturated solution of dimethylamine in 1 liter of tetrahydrofuran and the mixture stirred for 2 days at 25°. It is diluted with diethyl ether, washed with 2N aqueous sodium hydroxide, the organic layer dried, evaporated, the residue distilled and the fraction boiling at 106°/12 mm Hg collected, to yield the N,N-dimethyl-4-chlorobenzylamine. The starting material is prepared washed with 2N aqueous sodium hydroxide the organic layer dried evaporated the residue distilled the fraction boiling at 106°/12 mm Hg collected
Source ID: ord-c7c5c7090f0a4b668bd82da953428560PubChem References
These sources are listed in the compound's public database record.
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