Reaction #1416257
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04276426
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The process described in Example 2 is repeated, except that 1.3 liters of methyldichlorosilane, 1.7 liters of 1-methylstyrene and 5 ml of the catalytic solution are substituted for the trichlorosilane, allyl chloride and catalytic solution and the process is carried out at a temperature of 140° C. instead of 120° C. About 97.9 mol percent of the methyldichlorosilane used is converted and 12.8 moles per hour of 2-phenyl-2-methylethyl (methyl) dichlorosilane are obtained having a purity of 97.2 percent by weight as determined by gas chromatography. is carried out at a temperature of 140° C. instead of 120° C
Source ID: ord-a9893f0bfb7241fdab297ba0c4e34031