1-methylpiperidine-2-thione

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 1-Methyl-2-piperidothione (1.29 g) was dissolved in acetone (10 ml) and treated with benzyl bromide (1.7 g). After allowing the mixture to stand for 3 hours at room temperature a solid formed and was filtered off, washed with acetone, and dried to give the title compound (1.9 g) mp 168°-7° C. (Found: C, 52.5; H, 6.3; N, 4.8. C13H18BrNS requires C, 52.0; H, 6.0; N, 4.7%). a solid formed was filtered off washed with acetone dried

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 1-Methyl-2-piperidothione (1.29 g) was dissolved in acetone (10 ml) and treated with benzyl bromide (1.7 g).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 1-Methyl-2-piperidothione (1.29 g) was dissolved in acetone (10 ml) and treated with benzyl bromide (1.7 g). After allowing the mixture to stand for 3 hours at room temperature a solid formed and was filtered off, washed with acetone, and dried to give the title compound (1.9 g) mp 168°-7° C. (Found: C, 52.5; H, 6.3; N, 4.8. C13H18BrNS requires C, 52.0; H, 6.0; N, 4.7%). a solid formed was filtered off washed with acetone dried