No renderable structure data available
CCCCCCCCClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 1-chlorooctane |
|---|---|
| IUPAC Name | — |
| CAS Number | 111-85-3 |
| Database ID | 8142 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
1-chlorooctane (CAS 111-85-3) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 8142
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-597710d27cf14aa5a8f485c6d19dd6faConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e4eda99eb5374334a9fdc81454365abdConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-bb1f01cb34ca44e49164bad048d1b6dfConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-15142693dad04dc89213b112f6bf5607Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2df665250a3146a881bf41312b8fb366Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-6b3f80f25dae43eab76b50601537dcb1Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-335a6524b7b647eab90d709b61d54daaConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-85211951c8aa4ec1967a53ed67e7b29dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a solution containing 1.77 g of 1-amino-2,3-dihydro-4,6-dimethyl-7-hydroxy-1H-indene and 2 ml of triethylamine in 100 ml of chloroform was added dropwise 2.23 g of octyl chloride at room temperature. Then the reaction micture was stirred at the same temperature for 4 hours. The reaction mixture was washed with a diluted hydrochloric acid, water, an aqueous solution saturated with sodium bicarbonate, water and an aqueous soluction saturated with sodium chloride in this order, then dried with anhydrous sodium sulfate. The solvent was removed by evaporation and the residue thus obtained was dissolved in ethanol, tna an ethanol saturated with hydrogen chloride gas was added thereto form a hydrochlodide. Recrysttallized form acetonitrile to obtain 0.49 g of 2,3-dihydro-1-octylamino-4,6-dimethyl-7-hydroxy-1H-indene hydrochloride. Colorless needle-like crystals. Melting point: 120°-121° C. The reaction mixture was washed with a diluted hydrochloric acid, water an aqueous solution saturated with sodium bicarbonate, water and an aqueous soluction saturated with sodium chloride in this order, then dried with anhydrous sodium sulfate The solvent was removed by evaporation the residue thus obtained was added thereto form a hydrochlodide
Source ID: ord-5c393ffbbf5f4ea1ae77778299073b47Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To a solution containing 1.77 g of 1-amino-2,3-dihydro-4,6-dimethyl-7-hydroxy-1H-indene and 2 ml of trethylamine in 100 ml of chloroform was added dropwise 2.23 g of octyl chloride at room temperature. Then the reaction mixture was stirred at the same temperature for 4 hours. The reaction mixture was washed with a diluted hydrochloric acid, water, an aqueous solution saturated with sodium bicarbonate, water and an aqueous solution saturated with sodium chloride in this order, then dried with anhydrous sodium sulfate. The solvent was removed by evaporation and the residue thus obtained was dissolved in ethanol, tna an ethanol saturated with hydrogen chloride gas was added thereto form a hydrochlodide. Recrysttallized form acetonitrile to obtain 0.49 g of 2,3-dihydro-1-octylamino-4,6-dimethyl-7-hydroxy-1H-indene hydrochloride. Colorless needle-like crystals. Melting point: 120°-121° C. The reaction mixture was washed with a diluted hydrochloric acid, water an aqueous solution saturated with sodium bicarbonate, water and an aqueous solution saturated with sodium chloride in this order, then dried with anhydrous sodium sulfate The solvent was removed by evaporation the residue thus obtained was added thereto form a hydrochlodide
Source ID: ord-c725f75b4fff4a20a8578d6414a24b61Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-597710d27cf14aa5a8f485c6d19dd6faConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e4eda99eb5374334a9fdc81454365abdPubChem References
These sources are listed in the compound's public database record.
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