lead(2+);octadecanoate

Conditions: temp:70.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Separately, 3.5 l of warm water maintained at 70° C. was charged in a stainless steel beaker having a capacity of 10 l, and 419 g of stearic acid was added and dissolved under heating. Then, 24.0 cc of 7 N aqueous ammonia was dropped to the solution and the mixture was stirred and homogeneously emulsified to form an ammonia soap liquid. Separately, 725 cc of a lead monoxide slurry (PbO-DS) having a concentration of 680 g/l, 1 l of water and 14.2 cc of acetic acid having a concentration of 2.7 moles/liter were charged in a high-speed stirrer-equipped stainless steel vessel having a capacity of 10 l, and the mixture was maintained at 70° C. The above-mentioned ammonia soap liquid was added to this lead monoxide slurry and reaction was carried out under agitation to form a lead stearate slurry. were charged in a high-speed stirrer-equipped stainless steel vessel

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: A 500-ml capacity beaker was charged with 147 g of stearic acid and it was molten at 160°±5° C. in an oil bath under agitation by a glass vane, and 57.74 g of the lead monoxide powder (Sample A-6) and 0.31 g of powdery hydroxylamine sulfate were gradually added to the melt to effect reaction. Then, aging was conducted for 15 minutes to obtain a melt of lead stearate. The melt was poured into a watch glass and naturally cooled. The resulting solid was pulverized by an atomizer to obtain a lead stearate powder (Sample 2-7). were gradually added to the melt reaction

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 100.4 g of stearic acid and 83.0 g of lead oxide were stirred at 45° C. and 0.3% of acetic acid added. After stirring for 1 minute, slight clumping occurred. After cooling for 5 minutes, stirring was continued. A pale yellowish powder having a lead content of 40.9%, a melting temperature of 114° C., and an acid value of 2.0 was obtained after 20 minutes. After cooling for 5 minutes stirring a melting temperature of 114° C., and an acid value of 2.0 was obtained after 20 minutes

Conditions: temp:70.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: Separately, 3.5 l of warm water maintained at 70° C. was charged in a stainless steel beaker having a capacity of 10 l, and 419 g of stearic acid was added and dissolved under heating. Then, 24.0 cc of 7 N aqueous ammonia was dropped to the solution and the mixture was stirred and homogeneously emulsified to form an ammonia soap liquid. Separately, 725 cc of a lead monoxide slurry (PbO-DS) having a concentration of 680 g/l, 1 l of water and 14.2 cc of acetic acid having a concentration of 2.7 moles/liter were charged in a high-speed stirrer-equipped stainless steel vessel having a capacity of 10 l, and the mixture was maintained at 70° C. The above-mentioned ammonia soap liquid was added to this lead monoxide slurry and reaction was carried out under agitation to form a lead stearate slurry. were charged in a high-speed stirrer-equipped stainless steel vessel