Reaction #3873395
Related Literature (1)
openreactiondata ↗doi:10.1039/C8SC04228D
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-9661f42ae72a4de784496fd876c66c02No renderable structure data available
C1=CC=C2C(=C1)C(=CO2)CCNC=OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-[2-(1-benzofuran-3-yl)ethyl]formamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 100480-86-2 |
| Database ID | 13923851 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-[2-(1-benzofuran-3-yl)ethyl]formamide (CAS 100480-86-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 13923851
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-9661f42ae72a4de784496fd876c66c02Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2 N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-a25e39a8707c4822b86cd8e84a9fce96Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2 N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-a25e39a8707c4822b86cd8e84a9fce96Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-e3353796cc544f0db271fd22430ad475Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-e3353796cc544f0db271fd22430ad475Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-539c1345ae2040afb4f9022e288362d6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-539c1345ae2040afb4f9022e288362d6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4) , filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-ef7cbc829ce44fc89771a48e1bca533dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 grams (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 milliliters of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl extracted with methylene chloride, the latter washed with 5% sodium hydroxide, dried, filtered and concentrated to obtain the product. extracted with methylene chloride the latter washed with 5% sodium hydroxide dried filtered concentrated to obtain the product
Source ID: ord-4ac262eabca34b2da9776e6118807875Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 g (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (MgSO4), filtered and concentrated to give 2.70 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (MgSO4) filtered concentrated
Source ID: ord-9b18f248c70e4a0392e77af9b435df2fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 121 g of 2-(3-benzo[b]furanyl)-ethylamine and 300 mL of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl and washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v), dried (Na2SO4), charcoaled and concentrated to give 118 g of product. washed with methylene chloride which in turn was washed with 5% sodium hydroxide (w/v) dried (Na2SO4) concentrated
Source ID: ord-9f4fdd9381e043b59fde473ab24256e6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of 2.35 grams (0.015 mole) of 2-(3-benzo[b]furanyl)ethylamine and 5 milliliters of ethyl formate was heated at 60° C. for 3 hours, poured into 2N HCl extracted with methylene chloride, the latter washed with 5% sodium hydroxide, dried, filtered and concentrated to obtain the product. extracted with methylene chloride the latter washed with 5% sodium hydroxide dried filtered concentrated to obtain the product
Source ID: ord-46f07745db6c4d65a5d0c9b390d38e79PubChem References
These sources are listed in the compound's public database record.
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