No renderable structure data available
CC1(C(=CC(=O)O1)N2CCCC2)CChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2-one |
|---|---|
| IUPAC Name | — |
| CAS Number | 944591-46-2 |
| Database ID | 25247336 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
5,5-dimethyl-4-pyrrolidin-1-ylfuran-2-one (CAS 944591-46-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 25247336
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-3d434f141164459fb8cf3b250cc796f3Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-78b0883288cf4de68deadf6efa90fd01Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-6057f08f280d40e299280dbdc5fb3106Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-5f75305b2f2e40abb74ffdea41f99db7Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-78b0883288cf4de68deadf6efa90fd01Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-6057f08f280d40e299280dbdc5fb3106Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-6057f08f280d40e299280dbdc5fb3106Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-3d434f141164459fb8cf3b250cc796f3Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-f839309d7b244982b05d4c644c9d4f6bConditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-5f75305b2f2e40abb74ffdea41f99db7Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-78b0883288cf4de68deadf6efa90fd01Conditions: temp:88.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A suspension of 5,5-dimethyl-4-pyrrolidin-1-ylfuran-2(5H)-one (535 mg) in a mixture of MeOH (2 mL) and 5M HCl (8 mL) was heated at 88° C. for 2 hours. The mixture was cooled to room temp., extracted with CHCl3 (10×15 mL), combined, dried over Na2SO4, and evaporated to dryness to give 4-hydroxy-5,5-dimethyl-5H-furan-2-one as light brown solid. Yield: 359 mg, 95%. The mixture was cooled to room temp. extracted with CHCl3 (10×15 mL) dried over Na2SO4 evaporated to dryness
Source ID: ord-6057f08f280d40e299280dbdc5fb3106PubChem References
These sources are listed in the compound's public database record.
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