No renderable structure data available
CC1=C(C=CC(=C1)N)NC(=O)C2=CC=CC=C2FChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-(4-amino-2-methylphenyl)-2-fluorobenzamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 926204-38-8 |
| Database ID | 16775461 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-(4-amino-2-methylphenyl)-2-fluorobenzamide (CAS 926204-38-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 16775461
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e1770db3a72f4f4ca8a25bdc144d2c32Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-c5810c0bc1a442c7b4ac0fbfc1168e90Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-e1770db3a72f4f4ca8a25bdc144d2c32Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-2a6be3f89b83443d898839c2298af6cfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 40 C for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate cooled at 40 C for 12 hours Filtration
Source ID: ord-d0fc0b757bc34e1781ce138dd431b215Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 niL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 niL of ethyl acetate Filtration
Source ID: ord-32c9b879465648bb9ddcd7ad27d39838Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-6ae5bf86eb014fbd9f18577e04a538f3Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-4f914c7c314742328d6ed0df3c5e7ae3Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-5355cfd119b249a7a4bf816f3df0b2b1Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-dafc6104d0444c6e99ed4a9d765fafdbConditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-32aa993b4b4341f084a2c905ed1196d9Conditions: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration
Source ID: ord-64bdce1a00fd4fd5807deb718b6ef4daPubChem References
These sources are listed in the compound's public database record.
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