1,1,2,2-Tetrahydroperfluoro dodecanol

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In the same manner as in Example 1, except that 2-(perfluorodecyl)ethanol 16.9 g (0.03 mol) was used instead of 2-(perfluorooctyl)ethanol and the amount of 5% Pd-C (pH 6.8) to be added was 0.34 g, reaction was carried out to obtain the objective dodecyl{2-(perfluorodecyl)ethyl}ether 21.1 g (0.029 mol) as a white solid. Isolation yield was 96%. 0.34 g, reaction

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In the same manner as in Example 1, except that 2-(perfluorodecyl)ethanol 16.9 g (0.03 mol) was used instead of 2-(perfluorooctyl)ethanol and the amount of 5% Pd-C (pH 6.8) to be added was 0.34 g, reaction was carried out to obtain the objective dodecyl{2-(perfluorodecyl)ethyl}ether 21.1 g (0.029 mol) as a white solid. Isolation yield was 96%. 0.34 g, reaction

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: In the same manner as in Example 1, except that 2-(perfluorodecyl)ethanol 16.9 g (0.03 mol) was used instead of 2-(perfluorooctyl)ethanol and the amount of 5% Pd-C (pH 6.8) to be added was 0.34 g, reaction was carried out to obtain the objective dodecyl{2-(perfluorodecyl)ethyl}ether 21.1 g (0.029 mol) as a white solid. Isolation yield was 96%. 0.34 g, reaction