No renderable structure data available
CCOC(=O)C1C(C1(C)C)(C)CChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | ethyl 2,2,3,3-tetramethylcyclopropane-1-carboxylate |
|---|---|
| IUPAC Name | — |
| CAS Number | 771-10-8 |
| Database ID | 136614 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
ethyl 2,2,3,3-tetramethylcyclopropane-1-carboxylate (CAS 771-10-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 136614
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b6e69d3cdb58425883e6fe7150704a89Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-a2e60364939d4fdba49b783a1b493e85Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-84b9cb8ab27f4d2984f40276fd3c8cbfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-84b9cb8ab27f4d2984f40276fd3c8cbfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.). To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-dc58bb1051964ce99de7e47a877ccbdfConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.). To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-a395d2e5d0a745a991f9f24cb05b07faConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-a2e60364939d4fdba49b783a1b493e85Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-a2e60364939d4fdba49b783a1b493e85Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b6e69d3cdb58425883e6fe7150704a89Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-902a9ed269e14293bc9539d03a987c93Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.) To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-105f5ccfe85943db931b9a207605828dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The method of Mesheheryakov, Chem. Abstr., 54, 24436d (1960) was employed. To a mixture of 19 g. (0.226 mole) of 2,3-dimethyl-2-butene and 2 g. of cupric sulfate is added at reflux a mixture of 51 g. (0.447 mole) ethyl diazoacetate and 19 g. of 2,3-dimethyl-2-butene. The resulting mixture is heated at reflux for 3 hours, cooled, filtered and distilled to afford 19.8 g. (26%) of the desired cyclic ester, B.P. 76°-77° (15 mm.). To a mixture of 19 g at reflux a mixture of 51 g The resulting mixture is heated at reflux for 3 hours cooled filtered distilled to afford 19.8 g
Source ID: ord-369bd45ca37a429e995cf424b3b87a5cPubChem References
These sources are listed in the compound's public database record.
Related Products
12 related records
CAS 20602-89-5
CAS 113526-01-5
CAS 2907-92-8
CAS 54004-42-1
CAS 180573-21-1
CAS 54857-48-6
CAS 1515923-85-9
CAS 1461705-13-4
CAS 2985-35-5
CAS 41301-66-0
CAS 97935-32-5
CAS 249728-64-1
Request a Quote
Send the required specification, quantity, destination and intended use. The CATO team will review availability and respond.