N-ethylpiperazine-1-carboxamide

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared by the above procedure using 6-methoxy-1-indanone (2.4 g, 15 mmol), N-ethyl-1-piperazinecarboxamide (2.4 g, 15 mol), titanium(IV) isopropoxide (6 mL, 18 mmol) and sodium borohydride (2.7 g, 67 mmol) to give 2.8 g of product as the fumarate salt.