N,N-Dimethyl-2-iodoacetamide

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From N7-ethyl-4-methoxy-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 431 (M+H+, 100).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From 4-methoxy-N7-methyl-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 417 (M+H+, 100).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From N7-ethyl-4-methoxy-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 431 (M+H+, 100).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From 4-methoxy-N7-methyl-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 417 (M+H+, 100).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From N7-ethyl-4-methoxy-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 431 (M+H+, 100).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: From 4-methoxy-N7-methyl-benzothiazole-2,7-diamine with potassium carbonate and 2-iodo-N,N-dimethyl-acetamide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 417 (M+H+, 100).