methyl 3-amino-5-hydroxybenzoate

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The desired compound was prepared according to the procedure of Example D5, step B, using 2-({3-[(2,5-dichloropyrimidin-4-yl)amino]phenyl}thio)ethanol and methyl 3-amino-5-hydroxybenzoate as the starting materials in 99% yield. LCMS for C20H20ClN4O4S (M+H)+: m/z=446.9.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The desired compound was prepared according to the procedure of Example D5, step B, using 2-({3-[(2,5-dichloropyrimidin-4-yl)amino]phenyl}thio)ethanol and methyl 3-amino-5-hydroxybenzoate as the starting materials in 99% yield. LCMS for C20H20ClN4O4S (M+H)+: m/z=446.9.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The desired compound was prepared according to the procedure of Example D5, step B, using 2-({3-[(2,5-dichloropyrimidin-4-yl)amino]phenyl}thio)ethanol and methyl 3-amino-5-hydroxybenzoate as the starting materials in 99% yield. LCMS for C20H20ClN4O4S (M+H)+: m/z=446.9.