N-(thian-4-ylidene)hydroxylamine

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: By the same reaction and treatment as in Example 48 using tetrahydro-4H-thiopyran-4-one oxime and ethyl 4-(4-(4-chlorophenyl)piperazin-1-yl)-n-butyrate, 3-(3-(4-(4chlorophenyl)piperazin-1-yl)propyl)-6,7-dihydro-4H-thiopyrano[4,3-c]isoxazole is obtained.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: By the same reaction and treatment as in Example 48 using tetrahydro-4H-thiopyran-4-one oxime and ethyl 4-(4-(4-chlorophenyl)piperazin-1-yl)-n-butyrate, 3-(3-(4-(4chlorophenyl)piperazin-1-yl)propyl)-6,7-dihydro-4H-thiopyrano[4,3-c]isoxazole is obtained.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: By the same reaction and treatment as in Example 48 using tetrahydro-4H-thiopyran-4-one oxime and ethyl 4-(4-(4-chlorophenyl)piperazin-1-yl)-n-butyrate, 3-(3-(4-(4chlorophenyl)piperazin-1-yl)propyl)-6,7-dihydro-4H-thiopyrano[4,3-c]isoxazole is obtained.