No renderable structure data available
CC(C)COC(=O)C(C)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-methylpropyl 2-hydroxypropanoate |
|---|---|
| IUPAC Name | — |
| CAS Number | 585-24-0 |
| Database ID | 92814 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-methylpropyl 2-hydroxypropanoate (CAS 585-24-0) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 92814
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
11 reactions · 11 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2d2abf8c3d594dc499872acbf464b88aConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-09d382d603db45b58fcc4ca7cc9abf84Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-55c1dcb7f51a464e8199bd9ba12a93ceConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2d2abf8c3d594dc499872acbf464b88aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The composition of matter of 1-butyl lactate is and its preparation are disclosed in Gabriel et al. U.S. Pat. No. 1,668,806 (1928). They prepared 1-butyl lactate by dehydrating 70% lactic acid with excess 1-butanol at 117° C., followed by addition of HCl catalyst, followed by refluxing and esterification with addition excess 1-butanol and drawing a 1-butanol water azeotrope overhead. Nakanishi and Tsuda (Japanese Patent JP 46/30176 [71/30176]) consider production of 1-butyl lactate by extraction of an acidified crude fermentation broth with 1-butanol, followed by esterification of the extract phase. BASF (EP 159-285) considers production of isobutyl lactate by extraction of an acidified crude fermentation broth with isobutanol, followed by esterification of the extract phase, which was then distilled in vacuum 80° C./25 mbar to give a purified isobutyl lactate. its preparation at 117° C. by refluxing by extraction of by extraction of was then distilled in vacuum 80° C./25 mbar
Source ID: ord-5a37d7d15a7943c58ecb95b9ab25a852Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The composition of matter of 1-butyl lactate is and its preparation are disclosed in Gabriel et al. U.S. Pat. No. 1,668,806 (1928). They prepared 1-butyl lactate by dehydrating 70% lactic acid with excess 1-butanol at 117° C., followed by addition of HCl catalyst, followed by refluxing and esterification with addition excess 1-butanol and drawing a 1-butanol water azeotrope overhead. Nakanishi and Tsuda (Japanese Patent JP 46/30176 [71/30176]) consider production of 1-butyl lactate by extraction of an acidified crude fermentation broth with 1-butanol, followed by esterification of the extract phase. BASF (EP 159-285) considers production of isobutyl lactate by extraction of an acidified crude fermentation broth with isobutanol, followed by esterification of the extract phase, which was then distilled in vacuum 80° C./25 mbar to give a purified isobutyl lactate. its preparation at 117° C. by refluxing by extraction of by extraction of was then distilled in vacuum 80° C./25 mbar
Source ID: ord-5a37d7d15a7943c58ecb95b9ab25a852Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The composition of matter of 1-butyl lactate is and its preparation are disclosed in Gabriel et al. U.S. Pat. No. 1,668,806 (1928). They prepared 1-butyl lactate by dehydrating 70% lactic acid with excess 1-butanol at 117° C., followed by addition of HCl catalyst, followed by refluxing and esterification with addition excess 1-butanol and drawing a 1-butanol water azeotrope overhead. Nakanishi and Tsuda (Japanese Patent JP 46/30176 [71/30176]) consider production of 1-butyl lactate by extraction of an acidified crude fermentation broth with 1-butanol, followed by esterification of the extract phase. BASF (EP 159-285) considers production of isobutyl lactate by extraction of an acidified crude fermentation broth with isobutanol, followed by esterification of the extract phase, which was then distilled in vacuum 80° C./25 mbar to give a purified isobutyl lactate. its preparation at 117° C. by refluxing by extraction of by extraction of was then distilled in vacuum 80° C./25 mbar
Source ID: ord-5a37d7d15a7943c58ecb95b9ab25a852Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-09d382d603db45b58fcc4ca7cc9abf84Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-55c1dcb7f51a464e8199bd9ba12a93ceConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The composition of matter of 1-butyl lactate is and its preparation are disclosed in Gabriel et al. U.S. Pat. No. 1,668,806 (1928). They prepared 1-butyl lactate by dehydrating 70% lactic acid with excess 1-butanol at 117° C., followed by addition of HCl catalyst, followed by refluxing and esterification with addition excess 1-butanol and drawing a 1-butanol water azeotrope overhead. Nakanishi and Tsuda (Japanese Patent JP 46/30176 [71/30176]) consider production of 1-butyl lactate by extraction of an acidified crude fermentation broth with 1-butanol, followed by esterification of the extract phase. BASF (EP 159-285) considers production of isobutyl lactate by extraction of an acidified crude fermentation broth with isobutanol, followed by esterification of the extract phase, which was then distilled in vacuum 80° C./25 mbar to give a purified isobutyl lactate. its preparation at 117° C. by refluxing by extraction of by extraction of was then distilled in vacuum 80° C./25 mbar
Source ID: ord-5a37d7d15a7943c58ecb95b9ab25a852Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-55c1dcb7f51a464e8199bd9ba12a93cePubChem References
These sources are listed in the compound's public database record.
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