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C1CCSC(SC1)CClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-(chloromethyl)-1,3-dithiepane |
|---|---|
| IUPAC Name | — |
| CAS Number | 54237-86-4 |
| Database ID | 21545027 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-(chloromethyl)-1,3-dithiepane (CAS 54237-86-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 21545027
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
9 reactions · 9 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-94f9372e7e8f4b0398aff6e3e6d15f0dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl-1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-a9ce8b9c4988475f8e45a17a521b5c3cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl-1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-a9ce8b9c4988475f8e45a17a521b5c3cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl-1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-a9ce8b9c4988475f8e45a17a521b5c3cConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-94f9372e7e8f4b0398aff6e3e6d15f0dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A 40% by weight aqueous solution of methylamine (100 ml) and 2-chloromethyl-1,3-dithiepane (50 grams) are charged into a glass reaction vessel equipped with a mechanical stirrer. The reaction mixture is stirred for a period of about 18 hours. After this time sodium hydroxide (18 grams) is added with stirring over a period of about 3 hours. Stirring is then continued for an additional period of about 16 hours. The organic phase of the reaction mixture is then separated, is washed with aqueous potasssium carbonate and dried over anhydrous magnesium sulfate. The dried product is then distilled under reduced pressure to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-N-methylamine. equipped with a mechanical stirrer with stirring over a period of about 3 hours Stirring is then continued for an additional period of about 16 hours The organic phase of the reaction mixture is then separated is washed with aqueous potasssium carbonate dried over anhydrous magnesium sulfate The dried product is then distilled under reduced pressure
Source ID: ord-41e82b9e59284d889495bae0eea340c3Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl- 1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-99fe250e87b345728719f715cc527a79Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-8ebf7def23164dc6b5ec362d754b824bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2,6-Diethylaniline (75 grams), 2-chloromethyl-1,3-dithiepane (36.5 grams), potassium carbonate (34 grams) and dimethylformamide (75 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of about 18 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dithiepan-2-ylmethyl)-2,6-diethylaniline. equipped with a mechanical stirrer thermometer and reflux condenser The reaction mixture is heated at reflux for a period of about 18 hours After this time the mixture is filtered distilled
Source ID: ord-a9ce8b9c4988475f8e45a17a521b5c3cPubChem References
These sources are listed in the compound's public database record.
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