No renderable structure data available
CCNC1CCCCCC1Chemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | N-ethylcycloheptanamine |
|---|---|
| IUPAC Name | — |
| CAS Number | 45806-60-8 |
| Database ID | 13112620 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
N-ethylcycloheptanamine (CAS 45806-60-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 13112620
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
10 reactions · 10 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-bdab2f256a4a4761beb24caeb674e4c0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-ethylcycloheptylamine (21.15 g) was added with ice bath cooling to a mixture consisting of trichloromethylchloroformate (29.7 g) end ethyl acetate (300 ml). Thereafter, the temperature was gradually elevated and heated with refluxing for 6 hours. After distilling off the solvent, the obtained oil was distilled under reduced pressure to obtain N-cycloheptyl -N-ethylcarbamoyl chloride (17.20 g). b.p. 125°-128° C./4.0 mbar. cooling to a mixture heated with refluxing for 6 hours After distilling off the solvent the obtained oil was distilled under reduced pressure
Source ID: ord-8416a9392e9b4ae295053020ba1fc29eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-ethylcycloheptylamine (21.15 g) was added with ice bath cooling to a mixture consisting of trichloromethylchloroformate (29.7 g) end ethyl acetate (300 ml). Thereafter, the temperature was gradually elevated and heated with refluxing for 6 hours. After distilling off the solvent, the obtained oil was distilled under reduced pressure to obtain N-cycloheptyl -N-ethylcarbamoyl chloride (17.20 g). b.p. 125°-128° C./4.0 mbar. cooling to a mixture heated with refluxing for 6 hours After distilling off the solvent the obtained oil was distilled under reduced pressure
Source ID: ord-8416a9392e9b4ae295053020ba1fc29eConditions: temp:10.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium borohydride (3.78 g) was gradually added with ice bath cooling to a methanol (600 ml) solution of N-ethylidenecycloheptylamine (41.7 g) and agitated at 10° C. for 3 hours. Thereafter, the solvent was distilled off, followed by extraction with methylene chloride. Then, the extract was dried over anhydrous magnesium sulfate. Methylene chloride was distilled off and the obtained oil was distilled under reduced pressure to obtain N-ethylcycloheptylamine (35.96 g). b.p. 110°-113° C./26.6 mbar. Thereafter, the solvent was distilled off followed by extraction with methylene chloride Then, the extract was dried over anhydrous magnesium sulfate Methylene chloride was distilled off the obtained oil was distilled under reduced pressure
Source ID: ord-d81de3fe33234dcda1e1186d3256855bConditions: temp:10.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium borohydride (3.78 g) was gradually added with ice bath cooling to a methanol (600 ml) solution of N-ethylidenecycloheptylamine (41.7 g) and agitated at 10° C. for 3 hours. Thereafter, the solvent was distilled off, followed by extraction with methylene chloride. Then, the extract was dried over anhydrous magnesium sulfate. Methylene chloride was distilled off and the obtained oil was distilled under reduced pressure to obtain N-ethylcycloheptylamine (35.96 g). b.p. 110°-113° C./26.6 mbar. Thereafter, the solvent was distilled off followed by extraction with methylene chloride Then, the extract was dried over anhydrous magnesium sulfate Methylene chloride was distilled off the obtained oil was distilled under reduced pressure
Source ID: ord-d81de3fe33234dcda1e1186d3256855bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-ethylcycloheptylamine (21.15 g) was added with ice bath cooling to a mixture consisting of trichloromethylchloroformate (29.7 g) end ethyl acetate (300 ml). Thereafter, the temperature was gradually elevated and heated with refluxing for 6 hours. After distilling off the solvent, the obtained oil was distilled under reduced pressure to obtain N-cycloheptyl -N-ethylcarbamoyl chloride (17.20 g). b.p. 125°-128° C./4.0 mbar. cooling to a mixture heated with refluxing for 6 hours After distilling off the solvent the obtained oil was distilled under reduced pressure
Source ID: ord-8416a9392e9b4ae295053020ba1fc29eConditions: temp:10.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium borohydride (3.78 g) was gradually added with ice bath cooling to a methanol (600 ml) solution of N-ethylidenecycloheptylamine (41.7 g) and agitated at 10° C. for 3 hours. Thereafter, the solvent was distilled off, followed by extraction with methylene chloride. Then, the extract was dried over anhydrous magnesium sulfate. Methylene chloride was distilled off and the obtained oil was distilled under reduced pressure to obtain N-ethylcycloheptylamine (35.96 g). b.p. 110°-113° C./26.6 mbar. Thereafter, the solvent was distilled off followed by extraction with methylene chloride Then, the extract was dried over anhydrous magnesium sulfate Methylene chloride was distilled off the obtained oil was distilled under reduced pressure
Source ID: ord-d81de3fe33234dcda1e1186d3256855bConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-bdab2f256a4a4761beb24caeb674e4c0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-ethylcycloheptylamine (21.15 g) was added with ice bath cooling to a mixture consisting of trichloromethylchloroformate (29.7 g) end ethyl acetate (300 ml). Thereafter, the temperature was gradually elevated and heated with refluxing for 6 hours. After distilling off the solvent, the obtained oil was distilled under reduced pressure to obtain N-cycloheptyl -N-ethylcarbamoyl chloride (17.20 g). b.p. 125°-128° C./4.0 mbar. cooling to a mixture heated with refluxing for 6 hours After distilling off the solvent the obtained oil was distilled under reduced pressure
Source ID: ord-8416a9392e9b4ae295053020ba1fc29eConditions: temp:10.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Sodium borohydride (3.78 g) was gradually added with ice bath cooling to a methanol (600 ml) solution of N-ethylidenecycloheptylamine (41.7 g) and agitated at 10° C. for 3 hours. Thereafter, the solvent was distilled off, followed by extraction with methylene chloride. Then, the extract was dried over anhydrous magnesium sulfate. Methylene chloride was distilled off and the obtained oil was distilled under reduced pressure to obtain N-ethylcycloheptylamine (35.96 g). b.p. 110°-113° C./26.6 mbar. Thereafter, the solvent was distilled off followed by extraction with methylene chloride Then, the extract was dried over anhydrous magnesium sulfate Methylene chloride was distilled off the obtained oil was distilled under reduced pressure
Source ID: ord-d81de3fe33234dcda1e1186d3256855bPubChem References
These sources are listed in the compound's public database record.
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