No renderable structure data available
CCCCCCCCC1CC(=O)OC1=OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 3-octyloxolane-2,5-dione |
|---|---|
| IUPAC Name | — |
| CAS Number | 4200-92-4 |
| Database ID | 77869 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
3-octyloxolane-2,5-dione (CAS 4200-92-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 77869
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
10 reactions · 10 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-d34661fefb9c4e88a1e832f5cb00fb7bConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 3-(3,5-di-t-butyl-4-hydroxyphenyl)propanoic acid hydrazide (12.1 g, 41.1 mmol), 2-octylsuccinic anhydride (9.0 g, 41.1 mmol) and 20 ml of toluene was refluxed for one hour under a nitrogen atmosphere with the azeotropic removal of water (Dean-Stark assembly). The solvent was removed under vacuum while heating the reaction mass. 18.7 g of a very viscous, clear yellow liquid was obtained. The solvent was removed under vacuum while heating the reaction mass 18.7 g of a very viscous, clear yellow liquid was obtained
Source ID: ord-ab3a76dd6a5f497d8b51714bca0ecc08Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 3-(3,5-di-t-butyl-4-hydroxyphenyl)propanoic acid hydrazide (12.1 g, 41.1 mmol), 2-octylsuccinic anhydride (9.0 g, 41.1 mmol) and 20 ml of toluene was refluxed for one hour under a nitrogen atmosphere with the azeotropic removal of water (Dean-Stark assembly). The solvent was removed under vacuum while heating the reaction mass. 18.7 g of a very viscous, clear yellow liquid was obtained. The solvent was removed under vacuum while heating the reaction mass 18.7 g of a very viscous, clear yellow liquid was obtained
Source ID: ord-ab3a76dd6a5f497d8b51714bca0ecc08Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 10 parts n-octylsuccinic anhydride and 12 parts tris(hydroxymethyl)aminomethane were heated neat 3 hrs. at 180° C. under a rapid flow of N2. The product was obtained as a colorless glass in 100% yield. The following spectral properties confirm the structure shown below: ir (neat) 3300 (OH), 1600 (C=N); nmr (CDCl3) δ 4.40 (broad s, 4.0 H, 2 CH2 's in rings), δ 4.25 (broad s, 3.7 H, 4 OH, addition of D2O eliminates peak), δ 3.55 (broadened 10 Hz AB, 7.2 H, 4 CH2O), δ 2.5 (broad s, 3.0 H, CH--CH), δ 1.4 (broad s with t shoulder at 0.9, 17 H, n-C8H17). at 180° C. The product was obtained as a colorless glass in 100% yield
Source ID: ord-91a820020d334e1496a06012f7e856f9Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 10 parts n-octylsuccinic anhydride and 12 parts tris(hydroxymethyl)aminomethane were heated neat 3 hrs. at 180° C. under a rapid flow of N2. The product was obtained as a colorless glass in 100% yield. The following spectral properties confirm the structure shown below: ir (neat) 3300 (OH), 1600 (C=N); nmr (CDCl3) δ 4.40 (broad s, 4.0 H, 2 CH2 's in rings), δ 4.25 (broad s, 3.7 H, 4 OH, addition of D2O eliminates peak), δ 3.55 (broadened 10 Hz AB, 7.2 H, 4 CH2O), δ 2.5 (broad s, 3.0 H, CH--CH), δ 1.4 (broad s with t shoulder at 0.9, 17 H, n-C8H17). at 180° C. The product was obtained as a colorless glass in 100% yield
Source ID: ord-91a820020d334e1496a06012f7e856f9Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 3-(3,5-di-t-butyl-4hydroxyphenyl)propanoic acid hydrazide (I2.1 g, 41.1 mmol), 2-octylsuccinic anhydride (9.0 g, 41.1 mmol) and 20 ml of toluene was refluxed for one hour under a nitrogen atmosphere with the azeotropic removal of water (Dean-Stark assembly). The solvent was removed under vacuum while heating the reaction mass. 18.7 g of a very viscous, clear yellow liquid was obtained. The solvent was removed under vacuum while heating the reaction mass 18.7 g of a very viscous, clear yellow liquid was obtained
Source ID: ord-421bfa608e6349619b5baf0486d61c63Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: n-Octylsuccinyl dichloride was prepared by reacting n-octylsuccinic anhydride with PCl5 at 105°-110° C. for about four hours. After working the product up 101.3 g of liquid was obtained which had a purity of 84.3% according to chloride content. The corrected yield was 79.2%. at 105°-110° C. for about four hours was obtained which
Source ID: ord-7a5f942dfdec4f5b9ca667a9f9c5440cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: n-Octylsuccinyl dichloride was prepared by reacting n-octylsuccinic anhydride with PCl5 at 105°-110° C for about four hours. After working the product up 101.3 g of liquid was obtained which had a purity of 84.3% according to chloride content. The corrected yield was 79.2%. at 105°-110° C for about four hours was obtained which
Source ID: ord-87e2ce8cd2ff404580f820793c426d82Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 3-(3,5-di-t-butyl-4-hydroxyphenyl)propanoic acid hydrazide (12.1 g, 41.1 mmol), 2-octylsuccinic anhydride (9.0 g, 41.1 mmol) and 20 ml of toluene was refluxed for one hour under a nitrogen atmosphere with the azeotropic removal of water (Dean-Stark assembly). The solvent was removed under vacuum while heating the reaction mass. 18.7 g of a very viscous, clear yellow liquid was obtained. The solvent was removed under vacuum while heating the reaction mass 18.7 g of a very viscous, clear yellow liquid was obtained
Source ID: ord-ab3a76dd6a5f497d8b51714bca0ecc08Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 10 parts n-octylsuccinic anhydride and 12 parts tris(hydroxymethyl)aminomethane were heated neat 3 hrs. at 180° C. under a rapid flow of N2. The product was obtained as a colorless glass in 100% yield. The following spectral properties confirm the structure shown below: ir (neat) 3300 (OH), 1600 (C=N); nmr (CDCl3) δ 4.40 (broad s, 4.0 H, 2 CH2 's in rings), δ 4.25 (broad s, 3.7 H, 4 OH, addition of D2O eliminates peak), δ 3.55 (broadened 10 Hz AB, 7.2 H, 4 CH2O), δ 2.5 (broad s, 3.0 H, CH--CH), δ 1.4 (broad s with t shoulder at 0.9, 17 H, n-C8H17). at 180° C. The product was obtained as a colorless glass in 100% yield
Source ID: ord-91a820020d334e1496a06012f7e856f9PubChem References
These sources are listed in the compound's public database record.
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