No renderable structure data available
C1=COC(=C1)CNC(=O)CClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-chloro-N-(furan-2-ylmethyl)acetamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 40914-13-4 |
| Database ID | 720922 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-chloro-N-(furan-2-ylmethyl)acetamide (CAS 40914-13-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 720922
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
9 reactions · 9 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-b479acb552034d01b197d963c532f7a4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-579f141a799349e98a55b521e785a4e5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-579f141a799349e98a55b521e785a4e5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwiseso that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-5bde5c864fc84686a5c88f89ebfe68fdConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-579f141a799349e98a55b521e785a4e5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
Source ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4PubChem References
These sources are listed in the compound's public database record.
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