01
Reaction #1392303
Reaction scheme
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Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US03965099
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Chloromethyl methyl carbonate (0.02 mol) is reacted with sodium 7-trifluoromethylmercaptoacetamido-3-(1-methyltetrazol-5-ylthiomethyl)-3-cephem-4-carboxylic acid (0.01 mol) in DMF for 20 hours. On work up as described in Example 1, methoxycarbonyloxymethyl 7-trifluoromethylmercaptoacetamido-3-(1-methyltetrazol-5-ylthiomethyl)-3-cephem-4-carboxylate is obtained.
Source ID: ord-495500dcb2e14f91a7d9233d0158e9c6