2-fluoro-N,N-Dimethyl aniline

Conditions: temp:120.01; pressure:0.00; stir:

Procedure: Prepared from 2-fluoro-N,N-dimethylaniline (1g, 27.8 mg, 0.200 mmol, 1.00 equiv) and catBH (36.0 mg, 0.300 mmol, 1.50 equiv) according to GP 1. The title compound was purified by flash column chromatography using cyclohexane/EtOAc/Et3N (30/1/1) as eluent to afford 3g (22.2 mg, 42%) as a white solid.